HIGH-YIELD SYNTHESIS OF THE PARENT C-UNSUBSTITUTED CALIX[4]RESORCINARENE OCTAMETHYL ETHER

被引：30

作者：

FALANA, OM ^{[1
]}

ALFARHAN, E ^{[1
]}

KEEHN, PM ^{[1
]}

STEVENSON, R ^{[1
]}

机构：

[1] BRANDEIS UNIV,DEPT CHEM,WALTHAM,MA 02254

来源：

TETRAHEDRON LETTERS | 1994年 / 35卷 / 01期

基金：

美国国家卫生研究院;

关键词：

D O I：

10.1016/0040-4039(94)88163-4

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Treatment of 2,4-dimethoxybenzyl alcohol with trifluoroacetic acid (TFA, 5% in CHCl3) affords, in almost quantitative yield calix[4]resorcinarene octamethyl ether, which on demethylation and acetylation yields the derived octa-acetate.

引用

页码：65 / 68

页数：4

共 15 条

[1] A SIMPLE SYNTHESIS OF CYCLOTRIBROMOVERATRYLENE (CTBV) - AN EXTRACTIVE OF THE RED ALGA HALOPYTIS-PINASTROIDES [J].

ALFARHAN, E ;

FALANA, OM ;

KEEHN, PM ;

STEVENSON, R .

TETRAHEDRON LETTERS, 1992, 33 (40) :5885-5886

[2] CYCLO-OLIGOMERIZATION OF VERATRYL ALCOHOL WITH TRIFLUOROACETIC-ACID [J].

ALFARHAN, E ;

KEEHN, PM ;

STEVENSON, R .

TETRAHEDRON LETTERS, 1992, 33 (25) :3591-3594

[3]

ALFARHAN E, 1992, J CHEM RES, V37, P36

[4]

BAYER A, 1882, BER, V5, P25

[5]

Caro N., 1892, BER DTSCH CHEM GES, V25, P939, DOI [10.1002/cber.189202501147, DOI 10.1002/CBER.189202501147]

[6]

ERDTMAN H, 1968, TETRAHEDRON LETT, P1679

[7]

Gutsche C. D., 1989, MONOGRAPHS SUPRAMOLE

[8]

HOGBERG AGS, 1980, J AM CHEM SOC, V102, P6046

[9]

KENT JA, 1974, RIEGELS HDB IND CHEM, P818

[10] The condensation of oxyhydro quinone with aldehydes [Second announcement] [J].

Liebermann, C ;

Lindenbaum, S .

BERICHTE DER DEUTSCHEN CHEMISCHEN GESELLSCHAFT, 1904, 37 :2728-2737

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