FLOW-INJECTION EXTRACTION SPECTROPHOTOMETRIC DETERMINATION OF SALBUTAMOL BY OXIDATIVE COUPLING WITH 4-AMINO-N,N-DIMETHYLANILINE

被引：0

作者：

BURNS, DT ^{[1
]}

CHIMPALEE, N ^{[1
]}

CHIMPALEE, D ^{[1
]}

LEIWONGCHAROEN, K ^{[1
]}

机构：

[1] SILPAKORN UNIV,FAC SCI,DEPT CHEM,NAKOM PATHOM 73000,THAILAND

来源：

ANALYTICA CHIMICA ACTA | 1992年 / 260卷 / 01期

关键词：

FLOW SYSTEM; SPECTROPHOTOMETRY; EXTRACTION; SALBUTAMOL;

D O I：

暂无

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Salbutamol can be determined spectrophotometrically at 605 nm after flow-injection extraction into chloroform after oxidative coupling with 4-amino-N,N-dimethylaniline. The carrier stream is distilled water and the reagents streams contain 5% (w/v) sodium hydrogencarbonate, 0.5% (w/v) potassium hexacyanoferrate(III) and 0.1% (w/v) 4-amino-N,N-dimethylanilinium sulphate. The sampling rate is 20 h-1. The calibration graph is linear up to 20.0-mu-g ml-1 salbutamol, based on injection volume 100-mu-l. The relative standard deviation (n = 10) was 1.9% for 10-mu-g ml-1 salbutamol. The system has been applied to the determination of salbutamol in pharmaceutical formulations.

引用

页码：65 / 68

页数：4

共 48 条

[31] SPECTROPHOTOMETRIC DETERMINATION OF CALCIUM WITH DICYCLOHEXANO-24-CROWN-8 AND PROPYL ORANGE BY SOLVENT-EXTRACTION FLOW-INJECTION METHOD [J].

MOTOMIZU, S ;

OSHIMA, M ;

YONEDA, N ;

IWACHIDO, T .

ANALYTICAL SCIENCES, 1990, 6 (02) :215-220

[32] Flow Injection Spectrophotometric Determination of N-Acetyl-L-cysteine as a Complex with Palladium(II) [J].

Giljanovic, Josipa ;

Brkljaca, Mia ;

Prkic, Ante .

MOLECULES, 2011, 16 (09) :7224-7236

[33] Flow-injection determination of chromium(III) by its catalysis on the oxidative coupling of 3-methyl-2-benzothiazolinone hydrazone with N-ethyl-N-(2-hydroxy-3-sulfopropyl)-3-methoxyaniline [J].

Kaneko, M ;

Kurihara, M ;

Nakano, S ;

Kawashima, T .

ANALYTICA CHIMICA ACTA, 2002, 474 (1-2) :167-176

[34] FLOW INJECTION SPECTROPHOTOMETRIC DETERMINATION OF N-ACETYLCYSTEINE AND CAPTOPRIL EMPLOYING PRUSSIAN BLUE GENERATION REACTION [J].

Suarez, Willian Toito ;

Pessoa-Neto, Osmundo Dantas ;

Janegitz, Bruno Campos ;

Vieira, Heberth Juliano ;

Faria, Ronaldo Censi ;

Fatibello-Filho, Orlando .

ANALYTICAL LETTERS, 2011, 44 (14) :2394-2405

[35] 2-(5-Nitro-2-Pyridylazo)-5-(N-Propyl-N-Sulfopropylamino)Phenol as a new analytical reagent for flow-injection spectrophotometric determination of trace vanadium(V) [J].

Takeshi Yamane ;

Yuzuru Yamaguchi .

Microchimica Acta, 1998, 130 :111-115

[36] 2-(5-nitro-2-pyridylazo)-5-(N-propyl-N-sulfopropylamino)phenol as a new analytical reagent for flow-injection spectrophotometric determination of trace vanadium(V) [J].

Yamane, T ;

Yamaguchi, Y .

MIKROCHIMICA ACTA, 1998, 130 (1-2) :111-115

[37] Flow-injection spectrophotometric determination of albumin in spinal fluid with 5,10,15,20-tetrakis(4-sulfonatophenyl)porphine [J].

Igarashi, S ;

Takahata, K ;

Nakamura, J ;

Sudo, T .

BUNSEKI KAGAKU, 1997, 46 (12) :995-998

[38] Spectrophotometric determination of vanadium(IV, V) in chloride-rich samples by its catalytic effect on the oxidative coupling of N,N-diphenylhydrazine with chromotropic acid [J].

Nakano, Shigenori ;

Matumoto, Yuko ;

Fukumoto, Yumi ;

Hayashi, Mikio .

MICROCHIMICA ACTA, 2009, 164 (1-2) :211-216

[39] SPECTROPHOTOMETRIC DETERMINATION OF MERCURY WITH 5,10,15,20-TETRAKIS(3-CHLORO-4-SULFOPHENYL)PORPHINE BY FLOW-INJECTION ANALYSIS [J].

PENG, XJ ;

MAO, QK ;

CHENG, JK .

MIKROCHIMICA ACTA, 1994, 113 (1-2) :81-89

[40] Flow-injection photometric determination of manganese(II) based on its catalysis of the periodate oxidation of N,N'-bis(2-hydroxy-3-sulfopropyl)tolidine [J].

Nakano, S ;

Matumoto, Y ;

Yoshii, M .

TALANTA, 2005, 68 (02) :312-317

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