SUPERCRITICAL FLUID EXTRACTION AND CLEANUP PROCEDURES FOR DETERMINATION OF XENOBIOTICS IN BIOLOGICAL SAMPLES

被引:36
作者
NAM, KS [1 ]
KAPILA, S [1 ]
YANDERS, AF [1 ]
PURI, RK [1 ]
机构
[1] UNIV MISSOURI,ENVIRONM TRACE SUBST RES CTR,COLUMBIA,MO 65203
关键词
D O I
10.1016/0045-6535(90)90195-Y
中图分类号
X [环境科学、安全科学];
学科分类号
08 ; 0830 ;
摘要
Application of supercritical carbon dioxide for rapid extraction of various xenobiotics from biological tissue and fluid samples was investigated. The results obtained indicate that good recoveries (≥ 80%) can be readily obtained for all but polar solutes (kOW ≤ 2.5). © 1990.
引用
收藏
页码:873 / 880
页数:8
相关论文
共 50 条
[31]   Derivatization procedures for gas chromatographic mass spectrometric determination of xenobiotics in biological samples, with special attention to drugs of abuse and doping agents [J].
Segura, J ;
Ventura, R ;
Jurado, C .
JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 1998, 713 (01) :61-90
[32]   HRMS for the quantification of xenobiotics in biological samples [J].
Yan, Yingfei ;
Du, Zhifeng ;
Jiang, Hongliang .
BIOANALYSIS, 2017, 9 (24) :1939-1941
[33]   ENVIRONMENTAL TRACE ANALYSIS OF SOLID SAMPLES WITH SUPERCRITICAL FLUID EXTRACTION [J].
LOHLEIT, M ;
BACHMANN, K .
FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 1989, 334 (07) :658-658
[34]   Optimization of supercritical fluid extraction of phenol and cresols in soil samples [J].
Llompart, MP ;
Lorenzo, RA ;
Cela, R .
JOURNAL OF CHROMATOGRAPHY A, 1996, 723 (01) :123-134
[35]   SUPERCRITICAL-FLUID EXTRACTION OF SULFONYLUREA HERBICIDES IN SOIL SAMPLES [J].
BERDEAUX, O ;
DEALENCASTRO, LF ;
GRANDJEAN, D ;
TARRADELLAS, J .
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1994, 56 (02) :109-117
[36]   Supercritical fluid extraction of analytes from environmental samples - A review [J].
Barnabas, I.J. ;
Dean, J.R. ;
Owen, S.P. .
Analyst, 1994, 119 (11) :2381-2394
[37]   Assessment of supercritical fluid extraction of pentachlorophenol from aqueous samples [J].
Aranda, R ;
Kruus, P .
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1997, 68 (01) :59-67
[38]   Supercritical fluid extraction for the analysis of pesticide residues in miscellaneous samples [J].
Motohashi, N ;
Nagashima, H ;
Párkányi, C .
JOURNAL OF BIOCHEMICAL AND BIOPHYSICAL METHODS, 2000, 43 (1-3) :313-328
[39]   Supercritical fluid extraction as a cleanup technique for gas chromatographic analysis of pesticides in wool wax [J].
Jones, FW .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1997, 45 (07) :2569-2572
[40]   Supercritical fluid extraction of actinides and heavy metals for environmental cleanup: A process development perspective [J].
Lin, YH ;
Smart, NG .
SUPERCRITICAL CARBON DIOXIDE: SEPARATIONS AND PROCESSES, 2003, 860 :23-35