Separation of arenols from a high-temperature coal tar

被引:18
|
作者
Yao, Ting [1 ]
Zong, Zhi-Min [1 ]
Wen, Zhe [1 ]
Mukasa, Robert [1 ]
Yuan, Nan-Hua [2 ]
Wei, Xian-Yong [1 ]
机构
[1] China Univ Min & Technol, Key Lab Coal Proc & Efficient Utilizat, Minist Educ, Xuzhou 221008, Peoples R China
[2] Panzhihua Coal Corp, Coking Co Ltd, Panzhihua 617016, Peoples R China
关键词
Coal tar; Arenols; Column chromatography; Identification; GC/MS analysis;
D O I
10.1016/j.ijmst.2011.09.002
中图分类号
TD [矿业工程];
学科分类号
0819 ;
摘要
A high-temperature coal tar collected from Xuzhou Coking Plant, Saint-Gobain Pipelines (Xuzhou) Co., Ltd. was exhaustively extracted with petroleum ether (PE). The extract was sequentially eluted through silica gel with PE and PE/ethyl acetate (EA) mixed solvents (volume ratio 2: 1) to afford two eluted fractions. The extract and eluted fractions were analyzed with gas chromatography/mass spectrometry. In total, 14 arenols were detected, including phenol, cresols, xylenols, fluorenols, phenanthren-3-ol and pyren-1-ol. (C) 2012 Published by Elsevier B.V. on behalf of China University of Mining & Technology.
引用
收藏
页码:243 / 244
页数:2
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