Separation of Iridoids By Vacuum Liquid Chromatography

被引：7
作者：
Handjieva, Nedjalka [1 ]
Saadi, Houcine [1 ]
Popov, Simeon [1 ]
Baranovska, Iskra [2 ]
机构：
[1] Bulgarian Acad Sci, Ctr Phytochem, Inst Organ Chem, BU-1113 Sofia, Bulgaria
[2] Inst Foreign Students, Sofia, Bulgaria
来源：
PHYTOCHEMICAL ANALYSIS | 1991年 / 2卷 / 03期
关键词：
Iridoids; vacuum liquid chromatography; Valeriana officinalis; Centranthus ruber; Plantago media; Viburnum lantana; Gentiana punctata; Erythraea centaurium;
D O I：
10.1002/pca.2800020308
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Vacuum liquid chromatography (VLC) was used for the separation of iridoids isolated from Valeriana officinalis L. and Centranthus ruber D. C. (Valerianaceae), Plantago media L. (Plantaginaceaea), Viburnum lantana L. (Caprifoliaceae), Gentiana punctata L. and Erythraea centaurium Pers. (Gentianaceae). The advantages of the technique over preparative thin layer chromatography and open-column chromatography are discussed. Decapetaloside was isolated from V. lantana for the first time as were sweroside and swertiamarin from G. punctata. Florisil was used for the first time as an adsorbent for VLC.
引用
收藏
页码：130 / 133
页数：4
相关论文
共 11 条
  • [1] THE APPLICATION OF VACUUM LIQUID-CHROMATOGRAPHY TO THE SEPARATION OF TERPENE MIXTURES
    COLL, JC
    BOWDEN, BF
    [J]. JOURNAL OF NATURAL PRODUCTS, 1986, 49 (05): : 934 - 936
  • [2] El-Nagar J., 1980, J NAT PRODUCTS, V49, P649
  • [3] 2 IRIDOIDS FROM VIBURNUM-LANTANA
    HANDJIEVA, N
    BARANOVSKA, I
    MIKHOVA, B
    POPOV, S
    [J]. PHYTOCHEMISTRY, 1988, 27 (10) : 3175 - 3179
  • [4] IRIDOIDS FROM VIBURNUM-BETULIFOLIUM
    JENSEN, SR
    NIELSEN, BJ
    NORN, V
    [J]. PHYTOCHEMISTRY, 1985, 24 (03) : 487 - 489
  • [5] CHEMICAL IONIZATION MASS-SPECTROMETRY WITH AMINES AS REACTANT GASES .7. AMINE CHEMICAL IONIZATION MASS-SPECTROMETRY OF SOME IRIDOID AND SECOIRIDOID GLUCOSIDES
    MOLLOVA, NN
    HANDJIEVA, NV
    POPOV, SS
    [J]. ORGANIC MASS SPECTROMETRY, 1989, 24 (11): : 1001 - 1007
  • [6] Morton A., 1988, J CHROMATOGR, V450, P3
  • [7] SEPARATION OF DITERPENOID ALKALOID MIXTURES USING VACUUM LIQUID-CHROMATOGRAPHY
    PELLETIER, SW
    CHOKSHI, HP
    DESAI, HK
    [J]. JOURNAL OF NATURAL PRODUCTS, 1986, 49 (05): : 892 - 900
  • [8] PELLETIER SW, 1985, ADV MED PLANT RES, P153
  • [9] VACUUM LIQUID-CHROMATOGRAPHY AND QUANTITATIVE H-1-NMR SPECTROSCOPY OF TUMOR-PROMOTING DITERPENE ESTERS
    PIETERS, LAC
    VLIETINCK, AJ
    [J]. JOURNAL OF NATURAL PRODUCTS, 1989, 52 (01): : 186 - 190
  • [10] IRIDOIDS FROM PLANTAGO-MEDIA
    SAADI, H
    HANDJIEVA, N
    POPOV, S
    EVSTATIEVA, L
    [J]. PHYTOCHEMISTRY, 1990, 29 (12) : 3938 - 3939
12