(E)-1-{4-[Bis(4-bromophenyl)methyl]-piperazin-1-yl}-3-(4-methylphenyl)prop-2-en-1-one

被引：0

作者：

Zhong, Yan ^{[1
]}

Zhang, XiaoPing ^{[2
]}

Wu, Bin ^{[3
]}

机构：

[1] Southeast Univ, Sch Chem & Chem Engn, Nanjing 210096, Jiangsu, Peoples R China

[2] Nanjing Med Univ, Ctr Lab Anim, Nanjing 210029, Jiangsu, Peoples R China

[3] Nanjing Med Univ, Sch Pharm, Hanzhong Rd 140, Nanjing 210029, Jiangsu, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

data-to-parameter ratio = 15.4; mean σ(C-C) = 0.012 Å; R factor = 0.075; single-crystal X-ray study; T = 293 K; wR factor = 0.155;

D O I：

10.1107/S1600536812003820

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C 27H 26Br 2N 2O, the piperazine ring adopts a chair conformation with the N - C bonds in equatorial orientations. The C=C double bond has an E configuration. The dihedral angle between the bromobenzene rings is 83.0 (4)°. In the crystal, inversion dimers linked through pairs of C - H⋯O hydrogen bonds generate R 2 2(10) loops.

引用

页码：O605 / U1423

页数：9

共 50 条

[21] (2E)-1-(2,4-Dichlorophenyl)-3-[3-(4-nitrophenyl)-1-phenyl-1-H-pyrazol-4-yl]-prop-2-en-1-one [J].

Isloor, Arun M. ;

Malladi, Shridhar ;

Gerber, Thomas ;

van Brecht, Benjamin ;

Betz, Richard .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O616-U1505

[22] (E)-3-(9-Anthryl)-1-(4-fluorophenyl)-2-(4-nitro-1H-imidazol-1-yl)prop-2-en-1-one [J].

Wang, Xiao-Ling ;

Wang, Guang-Zhou ;

Geng, Rong-Xia ;

Zhou, Cheng-He .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :O320-U2073

[23] (E)-3-(4-Hydroxy-3-methoxyphenyl)-1(4-hydroxyphenyl) prop-2-en-1-one [J].

Sathya, S. ;

Jonathan, D. Reuben ;

Prathebha, K. ;

Usha, G. ;

Jovita, J. .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 :O593-+

[24] (2E)-3-[4-(Benzyloxy)phenyl]-1-(2,6-dichloro-3-fluorophenyl)prop-2-en-1-one [J].

Praveen, Aletti S. ;

Yathirajan, Hemmige S. ;

Gerber, Thomas ;

van Brecht, Benjamin ;

Betz, Richard .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O3386-+

[25] (2E)-3-(4-Cyanophenyl)-1-(4,4 ''-difluoro-5 '-methoxy-1,1 ':3 ',1 ''-terphenyl-4 '-yl)-prop-2-en-1-one [J].

Fun, Hoong-Kun ;

Loh, Wan-Sin ;

Samshuddin, S. ;

Narayana, B. ;

Sarojini, B. K. .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O1877-+

[26] (E)-3-(2-Bromophenyl)-1-(3,4-dimethoxy-phenyl)prop-2-en-1-one [J].

Li, Zhe ;

Wang, Yanan ;

Peng, Kesong ;

Chen, Lingzi ;

Chu, Shenghui .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O776-U2544

[27] (2E)-1-(5-Chlorothiophen-2-yl)-3-(2,4,5-trimethoxyphenyl)prop-2-en-1-one [J].

Prabhu, A. N. ;

Jayarama, A. ;

Row, T. N. Guru ;

Upadhyaya, V. .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O2086-U959

[28] (E)-3-(2,4-Dimethoxyphenyl)-1-(3,4,5-trimethoxyphenyl)prop-2-en-1-one [J].

Wu, Jianzhang ;

Qiu, Junyan ;

Wu, Xiaokai ;

Yang, Shulin ;

Liu, Yonggen .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 :o154

[29] (E)-1-(3-Bromophenyl)-3-(3,4-dimethoxy-phenyl)prop-2-en-1-one [J].

Escobar, Carlos A. ;

Trujillo, Alexander ;

Howard, Judith A. K. ;

Fuentealba, Mauricio .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O887-U3295

[30] (2E)-1-(3,5-Dihydroxyphenyl)-3-(4-methoxyphenyl)prop-2-en-1-one [J].

Ezhilarasi, K. S. ;

Jonathan, D. Reuben ;

Sathya, Shanmugam ;

Prathebha, K. ;

Usha, G. .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 :O608-+

← 1 2 3 4 5 →