Crystal structure of 2,3-dihydronaphto[2,3-b] [1,5] dioxepin

被引:0
|
作者
Chaabane, TB [1 ]
Hadou, AO
Meganem, F
机构
[1] Fac Sci Bizerte, Lab Chim Inorgan & Structurale, Jarzouna 7021, Tunisia
[2] Fac Sci Bizerte, Organ Synth Lab, Jarzouna 7021, Tunisia
关键词
crystal structure; chemical synthesis; 2,3-dihydronaphto[2,3-b] [1,5] dioxepin;
D O I
10.1023/A:1011399416154
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The X-ray single crystal structure Of C13H12O2 compound was determined. It crystallizes in the orthorombic space group P2(1)2(1)2(1) with a = 7.8847(7), b = 9.639(1), c = 13.432(2) Angstrom, Z = 4 and V = 1020.8(3) Angstrom (3). The final R converged to 0.037 for 1763 independent reflexions. The title compound forms layers parallel to (1 0 0) planes and the three dimensional cohesion of the crystal is assumed by Van der Waals interactions. The molecule consists of two six-membered rings (A and B) and a seven-membered ring (C). A and B rings are planar, whereas the C ring has a chair conformation.
引用
收藏
页码:459 / 462
页数:4
相关论文
共 50 条
  • [21] SYNTHESIS AND PHARMACOLOGICAL ACTIVITY OF PYRROLO(2,3-B) QUINOLINE, PYRIDO(2,3-B) QUINOLINE AND AZEPINO(2,3-B) QUINOLINE DERIVATIVES
    ZHIDKOVA, AM
    GRANIK, VG
    GLUSHKOV, RG
    POLEZHAEVA, AI
    MASHKOVSKII, MD
    KHIMIKO-FARMATSEVTICHESKII ZHURNAL, 1976, 10 (05): : 18 - 22
  • [22] Synthesis of naphtho[2,3-b][1,4]dioxin, 2-substituted naphtho[2,3-b][1,4]dioxins and 2,3-disubstituted naphtho [2,3-b][1,4]dioxins
    Clavier, S
    Khouili, M
    Bouyssou, P
    Coudert, G
    TETRAHEDRON, 2002, 58 (08) : 1533 - 1540
  • [23] A convenient synthesis of dithieno[2,3-b] [2,3-h]quinolines and pyrimido [4′,5′:4,5]thieno [2,3-b]thieno[2,3-h]quinolines
    Geies, AA
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1999, 148 : 201 - 214
  • [24] 1,4-DIOXINO[2,3-B]PYRIDINES AND 1,4-OXATHIINO[2,3-B]PYRIDINES
    NEUNHOEFFER, H
    SPONHEIMER, O
    CHEMISCHE BERICHTE, 1990, 123 (12) : 2453 - 2454
  • [25] Chemistry of substituted quinolines:: Thieno[2,3-b] and thiopyrano[2,3-b]quinolines
    Kiran, Balaji M.
    Nandeshwarappa, Belalakatte P.
    Vaidya, Vijayavittala P.
    Mahadevan, Kittappa M.
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2007, 182 (05) : 969 - 980
  • [26] SYNTHESIS, STRUCTURE AND COMPARATIVE REACTIVITY OF HETEROAROMATIC BICYCLIC SYSTEMS OF 1-METHYLTHIENO(SELENOPHENO) [2,3-B]PYRROLE, THIENO(SELENOPHENO)[2,3-B]FURAN AND "THIENO(SELENOPHENO)[2,3-B]THIOPHENE
    KVITKO, IY
    SOKOLOVA, NB
    FRADKINA, SP
    ELTSOV, AV
    ZHURNAL ORGANICHESKOI KHIMII, 1976, 12 (07): : 1574 - 1585
  • [27] SIMPLE SYNTHESIS OF THIENO[2,3-B]PYRAZINE AND THIENO[2,3-B]PYRIDINE
    SCHNELLER, SW
    CLOUGH, FW
    HARDEE, LE
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1976, 13 (02) : 273 - 275
  • [28] SYNTHESIS OF THIAZOLO[2,3-B]BENZOTHIAZOLIUM AND THIAZOLO[2,3-B]BENZOXAZOLIUM SALTS
    KIM, DG
    MIRONOVA, IM
    AVDIN, VV
    IZVESTIYA VYSSHIKH UCHEBNYKH ZAVEDENII KHIMIYA I KHIMICHESKAYA TEKHNOLOGIYA, 1993, 36 (12): : 67 - 70
  • [29] Synthetic methods to insecticidalthieno [2,3-b] furans and furo[2,3-b] furans
    McCann, Stephen F.
    Hu, Yulin
    Hendrixson, Maura
    Coats, Reed A.
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2013, 246
  • [30] ELECTROCHEMICAL REDUCTION OF PYRIDO[2,3-B] PYRAZINES AND OF PYRAZINO[2,3-B] PYRAZINES
    ARMAND, J
    CHEKIR, K
    PINSON, J
    COMPTES RENDUS HEBDOMADAIRES DES SEANCES DE L ACADEMIE DES SCIENCES SERIE C, 1977, 284 (10): : 391 - 393