Crystal structure of 2,3-dihydronaphto[2,3-b] [1,5] dioxepin

被引：0
|
作者：
Chaabane, TB [1 ]
Hadou, AO
Meganem, F
机构：
[1] Fac Sci Bizerte, Lab Chim Inorgan & Structurale, Jarzouna 7021, Tunisia
[2] Fac Sci Bizerte, Organ Synth Lab, Jarzouna 7021, Tunisia
来源：
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2000年 / 30卷 / 07期
关键词：
crystal structure; chemical synthesis; 2,3-dihydronaphto[2,3-b] [1,5] dioxepin;
D O I：
10.1023/A:1011399416154
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The X-ray single crystal structure Of C13H12O2 compound was determined. It crystallizes in the orthorombic space group P2(1)2(1)2(1) with a = 7.8847(7), b = 9.639(1), c = 13.432(2) Angstrom, Z = 4 and V = 1020.8(3) Angstrom (3). The final R converged to 0.037 for 1763 independent reflexions. The title compound forms layers parallel to (1 0 0) planes and the three dimensional cohesion of the crystal is assumed by Van der Waals interactions. The molecule consists of two six-membered rings (A and B) and a seven-membered ring (C). A and B rings are planar, whereas the C ring has a chair conformation.
引用
收藏
页码：459 / 462
页数：4
相关论文
共 50 条
  • [1] Crystal structure of 2,3-dihydronaphto[2,3-b) [1,5] dioxepin
    T. Ben Chaabane
    A. Ould Hadou
    F. Meganem
    Journal of Chemical Crystallography, 2000, 30 (7) : 459 - 462
  • [2] 2,3-dihydronaphto[2,3-b][1,4]dioxine
    Cherni, SN
    Haloui, A
    Driss, A
    Meganem, F
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1998, 54 : 1865 - 1867
  • [3] Synthesis of pyrido[2,3-b][1,4] and [2,3-b][1,5] benzodiazepnes and their derivatives - A review
    Joshi, BC
    Chauhan, M
    INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 1996, 6 (02) : 157 - 164
  • [4] A SYNTHESIS OF PYRIDO[2,3-B][1,5]BENZODIAZEPINES
    OSMAN, AN
    ISMAIL, MM
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 1991, 30 (08): : 798 - 799
  • [5] Synthesis of thieno[2,3-b][1,5]benzoxazepine derivatives
    Kohara, T
    Tanaka, H
    Kimura, K
    Horiuchi, H
    Seio, K
    Arita, M
    Fujimoto, T
    Yamamoto, I
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2002, 39 (01) : 163 - 171
  • [6] A NOVEL SYNTHESIS OF PYRIDO[2,3-B][1,5]BENZODIAZEPINES
    OKAMOTO, Y
    ZAMA, Y
    TAKAGI, K
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1994, 31 (01) : 49 - 52
  • [7] 2,3-DIHYDROTHIAZOLO[2,3-B]QUINAZOLIN-5-1
    HOWARD, JC
    KLEIN, G
    JOURNAL OF ORGANIC CHEMISTRY, 1962, 27 (10): : 3701 - &
  • [8] NAPHTHO[1',2'-5,6]PYRANO[2,3-B][1,5]BENZODIAZEPINE DERIVATIVES
    ROMA, G
    ERMILI, A
    BALBI, A
    MASSA, E
    DIBRACCIO, M
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1981, 18 (08) : 1619 - 1623
  • [9] STRUCTURE OF 5-(1-METHYL-4-PIPERAZINYL)-[2,3-B][1,5]PYRIDO BENZOTHIAZEPINE
    SBIT, M
    DUPONT, L
    DIDEBERG, O
    LIEGEOIS, JF
    DELARGE, J
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1988, 44 : 319 - 321
  • [10] CRYSTAL AND MOLECULAR STRUCTURE OF 2-BROMOMETHYL-2,3-DIHYDROFURO[2,3-B]TROPONE
    SHIMANOU.H
    ASHIDA, T
    SASADA, Y
    KAKUDO, M
    MURATA, I
    KITAHARA, Y
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1967, 40 (04) : 779 - +
12345