Validation of high-performance liquid chromatography (HPLC) method for quantitative analysis of histamine in fish and fishery products

被引：16
|
作者：
Jinadasa, B. K. K. K. [1 ]
Jayasinghe, G. D. T. M. [1 ]
Ahmad, S. B. N. [1 ]
机构：
[1] Natl Aquat Resources Res & Dev Agcy NARA, IPHT, ACL, Crow Isl 15, Colombo, Sri Lanka
来源：
COGENT CHEMISTRY | 2016年 / 2卷
关键词：
high performance liquid chromatography (HPLC); histamine; method validation; fish;
D O I：
10.1080/23312009.2016.1156806
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A high-performance liquid chromatography method is described for quantitative determination and validation of histamine in fish and fishery product samples. Histamine is extracted from fish/fishery products by homogenizing with tri-chloro acetic acid, separated with Amberlite CG-50 resin and C18-ODS Hypersil reversed phase column at ambient temperature (25 degrees C). Linear standard curves with high correlation coefficients were obtained. An isocratic elution program was used; the total elution time was 10 min. The method was validated by assessing the following aspects; specificity, repeatability, reproducibility, linearity, recovery, limits of detection, limit of quantification and uncertainty. The validated parameters are in good agreement with method and it is a useful tool for determining histamine in fish and fishery products.
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页数：7
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