A SIMPLE ION-EXCHANGE CHROMATOGRAPHIC DETERMINATION OF NONVOLATILE ORGANIC-ACIDS IN SOME SPANISH EXOTIC FRUITS

被引：21

作者：

CANO, MP ^{[1
]}

TORIJA, E ^{[1
]}

MARIN, MA ^{[1
]}

CAMARA, M ^{[1
]}

机构：

[1] UNIV COMPLUTENSE MADRID,DEPT NUTR & FOOD SCI 2,E-28040 MADRID,SPAIN

来源：

ZEITSCHRIFT FUR LEBENSMITTEL-UNTERSUCHUNG UND-FORSCHUNG | 1994年 / 199卷 / 03期

关键词：

D O I：

10.1007/BF01193447

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

High-performance liquid chromatography (HPLC) permits accurate determination of non-volatile acids in fruit. The Spanish exotic fruits assayed were kiwi fruits (Actinidia chinensis), cvs Hayward, Bruno, Monty and Abbot; mangoes (Mangifera indica), cvs Smith and Lippens; papayas (Carica papaya), cv Solo; pineapples (Ananus comosus), cv Smooth Cayenne; and bananas (Musa cavendishii), cv Enana. Sample preparation for HPLC analysis basically consisted of methanol extraction, followed by an easy clean-up with a C18 cartridge. Separation of the different acids was accomplished using an ion-exchange column and detection was monitored at 214 nm. Reproducibility of the minor organic acids was quite acceptable, and the procedure described offers a rapid analytical alternative to gas chromatography. Oxalic, oxoglutaric, citric, galacturonic, tartaric, ascorbic, L-malic, quinic, succinic, fumaric and D-malic acids can be quantified by this method.

引用

页码：214 / 218

页数：5

共 50 条

[41] ION-EXCHANGE PAPER CHROMATOGRAPHIC RESOLUTION OF SOME RACEMIC DL-AMINO ACIDS ON ALGINATE [J].

AWAD, AMED ;

AWAD, OMED .

JOURNAL OF CHROMATOGRAPHY, 1974, 93 (02) :393-398

[42] GAS-CHROMATOGRAPHIC DETERMINATION OF AIRBORNE ORGANIC-ACIDS VIA THEIR ANILIDES [J].

VOHRA, K ;

GAIND, VS .

ANALYST, 1992, 117 (10) :1567-1570

[43] CHROMATOGRAPHIC INVESTIGATION OF CAROTENOIDS, SUGARS AND ORGANIC-ACIDS FROM DIOSPYROS-KAKI FRUITS [J].

DAOOD, HG ;

BIACS, P ;

CZINKOTAI, B ;

HOSCHKE, A .

FOOD CHEMISTRY, 1992, 45 (02) :151-155

[44] A NOTE ON THE DETERMINATION OF SOME ALKALI SALTS OF ORGANIC ACIDS BY ION EXCHANGE [J].

BLAUG, SM .

JOURNAL OF THE AMERICAN PHARMACEUTICAL ASSOCIATION, 1956, 45 (04) :274-275

[45] ENZYMATIC AND GAS-CHROMATOGRAPHIC DETERMINATION OF ORGANIC-ACIDS IN EGG PRODUCTS [J].

STUKE, T ;

DICKERTMANN, D ;

HILDEBRANDT, G .

ARCHIV FUR LEBENSMITTELHYGIENE, 1987, 38 (04) :103-106

[46] Ion chromatographic determination of some organic acids, chloride and phosphate in coffee and tea [J].

Alcázar, A ;

Fernández-Cáceres, PL ;

Martín, MJ ;

Pablos, F ;

González, AG .

TALANTA, 2003, 61 (02) :95-101

[47] ION-EXCHANGE CHROMATOGRAPHY OF ORGANIC-ACIDS USING A CHEMICALLY BONDED HYDROPHILIC ANION-EXCHANGE COLUMN WITH POTASSIUM BIPHTHALATE ELUENT [J].

SUZUKI, Y ;

KOIZUMI, H ;

TANI, K ;

DING, M .

BUNSEKI KAGAKU, 1991, 40 (01) :T15-T19

[48] INFLUENCE OF P-TRIFLUOROACETYLBENZOIC ACID-ESTERS ON SELECTIVITY IN ION-EXCHANGE EXTRACTION OF ANIONS OF ORGANIC-ACIDS [J].

AMPILOGOVA, NA ;

KARAVAN, VS ;

BELOSHAPKO, MI .

JOURNAL OF ANALYTICAL CHEMISTRY OF THE USSR, 1985, 40 (05) :715-719

[49] Ion Chromatographic Determination of Organic Acids and Cations via Exchange Columns Connected in Parallel [J].

丁明玉 ;

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ＳｕｚｕｋｉＹｏｓｈｉｈｉｔｏ .

TsinghuaScienceandTechnology, 1997, (04) :37-41

[50] ION-EXCHANGE CHROMATOGRAPHIC DETERMINATION OF LYSOZYME IN EGG-WHITE [J].

GALYEAN, RD ;

COTTERILL, OJ .

JOURNAL OF FOOD SCIENCE, 1981, 46 (06) :1827-&

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