EXPLOSIVE RESIDUE ANALYSIS BY CAPILLARY ELECTROPHORESIS AND ION CHROMATOGRAPHY

被引:80
作者
HARGADON, KA
MCCORD, BR
机构
[1] FED BUR INVEST ACAD,FED BUR INVEST LAB,CTR FORENS SCI RES & TRAINING,QUANTICO,VA 22135
[2] FED BUR INVEST LAB,MAT ANAL UNIT,WASHINGTON,DC 20535
来源
JOURNAL OF CHROMATOGRAPHY | 1992年 / 602卷 / 1-2期
关键词
D O I
10.1016/0021-9673(92)80087-B
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Capillary electrophoresis is investigated for application as a complementary technique to ion chromatography in the analysis of low-explosive residues. Detection limits, interference problems, and matrix effects are examined by comparing the use of ion chromatography and capillary electrophoresis in parallel analyses. The residue from several different types of explosive devices are examined, and the results show capillary electrophoresis to be a useful new technique in explosive analysis yielding good sensitivity, high resolution and short analysis times.
引用
收藏
页码:241 / 247
页数:7
相关论文
共 14 条
[1]  
BENDER EC, 1989, CRIME LAB DIGEST, V16, P78
[2]  
Conkling JA., 1985, CHEM PYROTECHNICS
[3]  
DEAN JA, 1985, LANGES HDB CHEM
[4]   FACTORS AFFECTING THE RESOLUTION AND DETECTABILITY OF INORGANIC ANIONS BY NON-SUPPRESSED ION CHROMATOGRAPHY [J].
GLATZ, JA ;
GIRARD, JE .
JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1982, 20 (06) :266-273
[5]   INDIRECT FLUORIMETRIC DETECTION AND QUANTIFICATION IN CAPILLARY ZONE ELECTROPHORESIS OF INORGANIC ANIONS AND NUCLEOTIDES [J].
GROSS, L ;
YEUNG, ES .
JOURNAL OF CHROMATOGRAPHY, 1989, 480 :169-178
[6]   INDIRECT FLUOROMETRIC DETECTION OF CATIONS IN CAPILLARY ZONE ELECTROPHORESIS [J].
GROSS, L ;
YEUNG, ES .
ANALYTICAL CHEMISTRY, 1990, 62 (05) :427-431
[7]   NEW METHOD OF BACKGROUND ELUENT CONDUCTIVITY ELIMINATION IN GRADIENT ION CHROMATOGRAPHY [J].
JANDIK, P ;
LI, JB ;
JONES, WR ;
GJERDE, DT .
CHROMATOGRAPHIA, 1990, 30 (9-10) :509-517
[8]   CONTROLLED CHANGES OF SELECTIVITY IN THE SEPARATION OF IONS BY CAPILLARY ELECTROPHORESIS [J].
JONES, WR ;
JANDIK, P .
JOURNAL OF CHROMATOGRAPHY, 1991, 546 (1-2) :445-458
[9]  
JONES WR, 1991, AM LAB MAY, P33
[10]  
REUTTER DJ, 1983, ANAL CHEM, V55, P1468