PREPARATION AND CHARACTERIZATION OF TRIS(1,10-PHENANTHROLINE) TECHNETIUM(III)

被引：11
作者：
KREMER, C
KREMER, E
机构：
[1] Catedra de Química Inorgánica, Facultad de Química, Montevideo
来源：
JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY-LETTERS | 1993年 / 175卷 / 06期
关键词：
D O I：
10.1007/BF02163748
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
The [Tc(phen)3](PF6)3 complex has been synthesized by ligand substitution on [Tc(tu)6]3+. The reaction proceeds quickly in aqueous solution. A pure compound is obtained with 40% yield. It was characterized by Tc elemental analysis, cerimetric titration, conductometry and electrophoresis. The corresponding spectroscopic properties (UV, Vis, IR and NMR) are also reported and discussed.
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页码：445 / 453
页数：9
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