5'-([1,1'-Biphenyl]-4-yl)-1',1",3"-tri-methyldispiro[indane-2,2'-pyrrolidine-4',5"-[1,3]diazinane]-1,3,2",4",6"-penta-one

被引：1

作者：

Subramanyahegde ^{[1
]}

Amar, Hosamani ^{[2
]}

Shivaraj, Yellappa ^{[1
]}

Vijayakumar, Giriyapura R. ^{[3
]}

Palakshamurthy, Bandrehalli Siddagangaiah ^{[4
]}

机构：

[1] Govt Sci Coll, Dept Chem, Bangalore 560001, Karnataka, India

[2] Indian Inst Sci, Solid State & Struct Chem Unit, Bangalore 560012, Karnataka, India

[3] Tumkur Univ, Dept Chem, UCS, Tumkur 572103, Karnataka, India

[4] Tumkur Univ, Dept Studies & Res Phys, UCS, Tumkur 572103, Karnataka, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷

关键词：

Data-to-parameter ratio = 13.2; Mean σ(C-C) = 0.003 Å; R factor = 0.050; Single-crystal X-ray study; T = 296 K; WR factor = 0.130;

D O I：

10.1107/S1600536814013117

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C30H25N3O5, the central five-membered heterocyclic ring adopts an envelope conformation, with the N atom as the flap. The dihedral angles between this central ring and the pendant indane ring system, the trione and benzene rings are 87.49 (5), 82.95 (10) and 72.42 (10)degrees, respectively. The dihedral angle between the rings of the biphenyl group is 45.99 (13)degrees. In the crystal, molecules are linked by C-H center dot center dot center dot O hydrogen bonds into [101] C(12) chains.

引用

页码：0759 / +

页数：10

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