COATING THE INSIDE OF A CAPILLARY OF SQUARE CROSS-SECTION

被引:138
作者
KOLB, WB [1 ]
CERRO, RL [1 ]
机构
[1] UNIV TULSA,DEPT CHEM ENGN,TULSA,OK 74104
关键词
D O I
10.1016/0009-2509(91)85119-I
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
Coating the walls of a capillary is usually done in two steps: (1) wetting or filling the capillary with a viscous fluid, and (2) clearing the capillary by forcing air through it. Clearing amounts to driving the wetting viscous fluid out of the capillary by another immiscible fluid. When air is blown into one end of a tube containing the viscous fluid, a "bubble" forms with the back end open. The bubble travels down the tube forcing some of the liquid out and leaving behind a fraction, in the form of a uniform film covering the walls. This paper reports flow visualization in capillaries of square cross section. Visualization of the bubble was done by viewing both side and diagonal planes of the capillary in order to analyze the effect of the square cross section. Measurements from the captured images were used to characterize the shape of the fluid-fluid interface. The coating thickness of liquid deposited on the capillary walls was measured as the fraction of the capillary volume occupied by the liquid. The results for a wide range of capillary numbers show that this fraction increased monotonically with increasing capillary number, approaching an asymptotic limit of 0.64. Sequential particle tracking techniques were used to determine the flow field in different regions surrounding the bubble. A semi-quantitative comparison of the flow behavior, in capillaries of square and circular cross section, has been carried out.
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页码:2181 / 2195
页数:15
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