HPLC AND GC METHODS FOR ANALYSIS OF WATER-SOLUBLE NITROSULFONIC ACIDS

被引：9

作者：

CROWLEY, TO ^{[1
]}

LARSON, RA ^{[1
]}

机构：

[1] UNIV ILLINOIS,INST ENVIRONM STUDIES,URBANA,IL 61801

来源：

JOURNAL OF CHROMATOGRAPHIC SCIENCE | 1994年 / 32卷 / 02期

关键词：

D O I：

10.1093/chromsci/32.2.57

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Two methods are reported for the analysis of nitrobenzene and nitrotoluene sulfonic acids. An ion-pairing solvent system containing cetyltrimethylammonium bromide for high-performance liquid chromatography is described; the method uses ultraviolet detection and nonpolar styrenedivinylbenzene columns. A gas chromatographic method that involves converting the sulfonic acid to an alkylamine derivative with a nucleophilic displacement reaction is also related. The latter method is most useful for highly nitrated compounds. © 1994 Oxford University Press.

引用

页码：57 / 60

页数：4

共 18 条

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