1-{(Z)-[2-Methoxy-5-(trifluoromethyl)anilino]methylidene}naphthalen-2(1H)one

被引：2

作者：

Kargili, Hakan ^{[1
]}

Agar, Aysen Alaman ^{[2
]}

Alpaslan, Goekhan ^{[3
]}

Bueyuekguengoera, Orhan ^{[1
]}

Erdoenmez, Ahmet ^{[1
]}

机构：

[1] Ondokuz Mayis Univ, Fac Arts & Sci, Dept Phys, TR-55139 Samsun, Turkey

[2] Ondokuz Mayis Univ, Fac Arts & Sci, Dept Chem, TR-55139 Samsun, Turkey

[3] Giresun Univ, Dept Med Serv & Techn, Vocat Sch Hlth Serv, TR-28200 Giresun, Turkey

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2013年 / 69卷

关键词：

data-to-parameter ratio = 12.1; disorder in main residue; mean σ(C-C) = 0.003 Å; R factor = 0.048; single-crystal X-ray study; T = 296 K; wR factor = 0.097;

D O I：

10.1107/S1600536812051410

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C19H14F3NO2, crystallizes in the ketoamine tautomeric form, with a strong intramolecular NH center dot center dot center dot O hydrogen bond. The molecule is almost planar; the dihedral angle between the naphthalene ring system and the benzene ring is 4.60 (7)degrees. In the crystal, molecules are linked into chains along the c axis by C-H center dot center dot center dot O hydrogen bonds. The F atoms of the trifluoromethyl group are disordered over two positions with refined site occupancies of 0.668 (9) and 0.332 (9).

引用

页码：O163 / +

页数：8

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