MEASUREMENT OF TRACE-ELEMENTS IN CERAMIC AND QUARTZ BY LASER ABLATION MICROWAVE-INDUCED PLASMA-ATOMIC EMISSION-SPECTROMETRY

被引:20
作者
CIOCAN, A [1 ]
HIDDEMANN, L [1 ]
UEBBING, J [1 ]
NIEMAX, K [1 ]
机构
[1] INST SPEKTROCHEM & ANGEW SPEKTROSKOPIE, BUNSEN KIRCHHOFF STR 11, W-4600 DORTMUND 1, GERMANY
关键词
LASER ABLATION; MICROWAVE-INDUCED PLASMA; ATOMIC EMISSION SPECTROMETRY; CERAMIC ANALYSIS; QUARTZ ANALYSIS;
D O I
10.1039/ja9930800273
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Laser ablation into a microwave induced plasma and atomic emission spectrometry of the plasma was applied to the direct determination of trace elements (magnesium, aluminium, silicon and iron) in a high-temperature superconducting ceramic (YBa2Cu3O7) and the determination of low sodium concentrations in high-purity natural and synthetic quartz used for the production of optical fibres. The emission spectra were measured by time-gated detection, normalized by internal standardization and calibrated with relevant spectra of standard reference samples (aluminium, copper and borax glass).
引用
收藏
页码:273 / 278
页数:6
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