SIMULTANEOUS DETERMINATION OF BARBITAL AND THIOBARBITURIC ACID BY DERIVATIVE SPECTROPHOTOMETRY

被引:6
作者
SORIANO, J [1 ]
JIMENEZ, F [1 ]
JIMENEZ, AI [1 ]
ARIAS, JJ [1 ]
机构
[1] UNIV LA LAGUNA,DEPT QUIM ANAL BROMATOL & TOXICOL,E-38204 LA LAGUNA,SPAIN
关键词
BARBITAL; THIOBARBITURIC ACID; DERIVATIVE SPECTROPHOTOMETRY; SIMULTANEOUS DETERMINATION;
D O I
10.1080/00387019208020691
中图分类号
O433 [光谱学];
学科分类号
0703 ; 070302 ;
摘要
A new method for the simultaneous determination of barbital and thiobarbituric acid by derivative spectrophotometry is proposed. The method allows the resolution of mixtures of the two components over the concentration ranges 0.37-4.70-mu-g/ml (barbital) and 0.40-4.50-mu-g/ml (thiobarbituric acid) provided the ratio between their concentrations does not exceed 5:1. It was applied to the determination of the two compounds in synthetic samples and blood serum.
引用
收藏
页码:257 / 270
页数:14
相关论文
共 13 条
[1]   2ND-DERIVATIVE SPECTROSCOPY OF PROTEINS - METHOD FOR QUANTITATIVE-DETERMINATION OF AROMATIC AMINO-ACIDS IN PROTEINS [J].
BALESTRIERI, C ;
COLONNA, G ;
GIOVANE, A ;
IRACE, G ;
SERVILLO, L .
EUROPEAN JOURNAL OF BIOCHEMISTRY, 1978, 90 (03) :433-440
[2]   DETERMINATION OF SOME CEPHALOSPORINS USING DERIVATIVE SPECTROPHOTOMETRY [J].
ELYAZBI, FA ;
BARARY, MH .
ANALYTICAL LETTERS PART B-CLINICAL AND BIOCHEMICAL ANALYSIS, 1985, 18 (05) :629-640
[3]   DETERMINATION OF CHLORPROMAZINE AND ITS SULFOXIDE IN PHARMACEUTICAL DOSAGE FORMS BY 3RD-ORDER DERIVATIVE ULTRAVIOLET SPECTROSCOPY [J].
FASANMADE, AA ;
FELL, AF .
ANALYST, 1985, 110 (09) :1117-1124
[4]   DOUBLE MODULATION ATOMIC FLUORESCENCE FLAME SPECTROMETRY [J].
FOWLER, WK ;
KNAPP, DO ;
WINEFORD.JD .
ANALYTICAL CHEMISTRY, 1974, 46 (04) :601-602
[5]   SIMULTANEOUS DETERMINATION OF HISTAMINE AND SPERMIDINE BY 2ND-DERIVATIVE SYNCHRONOUS FLUORESCENCE SPECTROMETRY [J].
GUTIERREZ, MC ;
RUBIO, S ;
GOMEZHENS, A ;
VALCARCEL, M .
ANALYTICA CHIMICA ACTA, 1987, 193 :349-354
[6]   SIMULTANEOUS 2ND-ORDER ANALOG DERIVATIVE SPECTROPHOTOMETRIC DETERMINATION OF VANADIUM AND COBALT IN STEELS [J].
JIMENEZ, AI ;
JIMENEZ, F ;
ARIAS, JJ .
ANALYST, 1989, 114 (01) :93-96
[7]   APPLICATION OF 2ND DERIVATIVE ULTRAVIOLET SPECTROMETRY .3. DETERMINATION OF EUGENOL, THYMOL AND ANETHOLE IN VOLATILE OILS [J].
KORANY, MA ;
ELDIN, AAS ;
ABDELSALAM, NA .
ANALYTICAL LETTERS PART A-CHEMICAL ANALYSIS, 1984, 17 (06) :483-495
[8]   1ST DERIVATIVE SPECTROPHOTOMETRIC DETERMINATION OF CERTAIN DRUGS IN 2-COMPONENT MIXTURES [J].
KORANY, MA ;
WAHBI, AM ;
ELSAYED, MA ;
MANDOUR, S .
ANALYTICAL LETTERS PART B-CLINICAL AND BIOCHEMICAL ANALYSIS, 1984, 17 (12) :1373-1389
[9]  
MCWILLIAMS IG, 1970, ANAL CHEM, V41, P674
[10]  
OHAVER TC, 1979, CLIN CHEM, V25, P1548