CONTINUOUS SOLVENT-EXTRACTION IN A CLOSED-LOOP SYSTEM

被引:33
作者
ATALLAH, RH [1 ]
RUZICKA, J [1 ]
CHRISTIAN, GD [1 ]
机构
[1] UNIV WASHINGTON, DEPT CHEM, CTR PROC ANALYT CHEM, BG 10, SEATTLE, WA 98195 USA
关键词
ORGANIC COMPOUNDS - ZINC COMPOUNDS;
D O I
10.1021/ac00151a015
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
An on-line continuous-flow solvent extraction system has been developed. The method consists of a segmentor, an extraction coil, a phase separator, a switching valve, and a pumping system. The performance of the system was illustrated by extracting copper with a solution of zinc diethyldithiocarbamate in chloroform. Parameters affecting proconcentration of the analyte in the system were examined. The method can be used for quantitative analysis and as a preparative technique.
引用
收藏
页码:2909 / 2914
页数:6
相关论文
共 26 条
[1]  
[Anonymous], SOLVENT EXTRACTION F
[2]  
ATALLAH RH, 1987, THESIS U WASHINGTON
[3]   PRECONCENTRATION AND MATRIX-ISOLATION OF HEAVY-METALS THROUGH A 2-STAGE SOLVENT-EXTRACTION IN A FLOW SYSTEM [J].
BENGTSSON, M ;
JOHANSSON, G .
ANALYTICA CHIMICA ACTA, 1984, 158 (02) :147-156
[4]   AUTOMATED SAMPLE PREPARATION [J].
BURNS, DA .
ANALYTICAL CHEMISTRY, 1981, 53 (12) :1403-&
[5]  
Charlot G, 1964, COLORIMETRIC DETERMI
[6]  
Chwastowska J., 1982, SEPARATION PRECONCEN
[7]  
DECASTRO MDL, 1986, J AUTOM CHEM, V8, P56, DOI 10.1155/S1463924686000135
[8]   AN EFFICIENT FLOW-INJECTION SYSTEM WITH ONLINE ION-EXCHANGE PRECONCENTRATION FOR THE DETERMINATION OF TRACE AMOUNTS OF HEAVY-METALS BY ATOMIC-ABSORPTION SPECTROMETRY [J].
FANG, ZL ;
RUZICKA, J ;
HANSEN, EH .
ANALYTICA CHIMICA ACTA, 1984, 164 (OCT) :23-39
[9]   ONLINE LIQUID-LIQUID-EXTRACTION IN A SEGMENTED FLOW DIRECTLY COUPLED TO ON-COLUMN INJECTION INTO A GAS-CHROMATOGRAPH [J].
FOGELQVIST, E ;
KRYSELL, M ;
DANIELSSON, LG .
ANALYTICAL CHEMISTRY, 1986, 58 (07) :1516-1520
[10]  
Foreman J. K., 1975, AUTOMATIC CHEM ANAL