Crystal structure of 1-[(6-chloropyridin-3-yl) sulfonyl]-1,2,3,4-tetrahydroquinoline

被引:2
|
作者
Jeyaseelan, S. [1 ]
Rajegowda, H. R. [2 ]
Rayan, R. Britto Dominic [3 ]
Kumar, P. Raghavendra [2 ]
Palakshamurthy, B. S. [4 ]
机构
[1] St Philomenas Coll Autonomous, Dept Phys, Mysore 570015, Karnataka, India
[2] Tumkur Univ, Dept Studies & Res Chem, Tumkur 572103, Karnataka, India
[3] St Philomenas Coll Autonomous, Dept Chem, Mysore 570015, Karnataka, India
[4] Tumkur Univ, Dept Studies & Res Phys, UCS, Tumkur 572103, Karnataka, India
关键词
crystal structure; 1,2,3,4-tetrahydroquinoline; C-H center dot center dot center dot O interactions; pharmacological activity;
D O I
10.1107/S2056989015008099
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The tetrahydropyridine ring of the quinoline system in the title compound, C14H13ClN2O2S, adopts a half-chair conformation with the bond-angle sum at the N atom being 350.0 degrees. The dihedral angle between the least-squares planes of the two aromatic rings is 50.13 (11)degrees. In the crystal, inversion dimers linked by pairs of C-H center dot center dot center dot O hydrogen bonds generate R-2(2) (10) loops. Additional intermolecular C-H center dot center dot center dot O hydrogen bonds generate C(7) chains along [100].
引用
收藏
页码:660 / +
页数:8
相关论文
共 50 条
  • [1] Crystal structure of 1-methanesulfonyl-1,2,3,4-tetrahydroquinoline
    Jeyaseelan, S.
    Babu, S. L. Nagendra
    Venkateshappa, G.
    Kumar, P. Raghavendra
    Palakshamurthy, B. S.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O20 - +
  • [2] Crystal structure of 1-benzylsulfonyl-1,2,3,4-tetrahydroquinoline
    Jeyaseelan, S.
    Sowmya, B. R.
    Venkateshappa, G.
    Kumar, P. Raghavendra
    Palakshamurthy, B. S.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O249 - U347
  • [3] 1-[(6-Chloropyridin-3-yl)methyl]-imidazolidin-2-one
    Kant, Rajni
    Gupta, Vivek K.
    Kapoor, Kamini
    Shripanavar, Chetan S.
    Banerjee, Kaushik
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1939 - +
  • [4] Syntheses and crystal structure of 4-[(pyridin-3yl)diazenyl]morpholine and 1-[(pyridin-3yl)diazenyl]-1,2,3,4-tetrahydroquinoline
    Sokhna, Seynabou
    Seck, Insa
    Thiam, Ibrahima El Hadj
    Presset, Marc
    Ndoye, Samba Fama
    Ba, Lalla Aicha
    Samb, Issa
    Coles, Simon
    Orton, James
    Seck, Matar
    Le Gall, Erwan
    Gaye, Mohamed
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2023, 79 : 74 - +
  • [5] 1-(3-DIETHYLAMINO-1-PROPYL)-6-METHOXY-1,2,3,4-TETRAHYDROQUINOLINE
    MCKEE, RL
    MCKEE, MK
    BOST, RW
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1947, 69 (02) : 471 - 471
  • [6] 1-[(6-Chloropyridin-3-yl)methyl]imidazolidin-2-iminium chloride
    Kant, Rajni
    Gupta, Vivek K.
    Kapoor, Kamini
    Deshmukh, Madhukar B.
    Shripanavar, Chetan S.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68
  • [7] 1-{6-(4-Chlorophenyl)-1-[(6-chloropyridin-3-yl)methyl]-2-[(6-chloropyridin-3-yl) methylsulfanyl]4-methyl-1,6-dihydropyrimidin-5-yl}ethanone
    Zhu, Xiao-Fei
    Shi, De-Qing
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O2506 - O2507
  • [8] INTERMOLECULAR REARRANGEMENT OF 1,2,3,4-TETRAHYDROQUINOLINE
    HAUSIGK, D
    TETRAHEDRON LETTERS, 1968, (24) : 2801 - &
  • [9] 1-[(6-Chloropyridin-3-yl)methyl]3-phenylimidazofidine-2,4-dione
    Ke Li
    De-Qing Shi
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3506 - U3464
  • [10] Theoretical study on the geometry and vibration of 1-{6-(4-Chlorophenyl)-1-[(6-chloropyridin-3-yl)methyl]-2-[(6-chloropyridin-3-yl)methylsulfanyl]-4-methyl-1,6-dihydropyrimidin-5-yl}ethanone
    Song, Yuanzhi
    Zhang, Lili
    HuiZhong
    Shi, Deqing
    Xie, Jimin
    Zhao, Ganqing
    SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2008, 70 (04) : 943 - 952