TIME AND TEMPERATURE RESOLVED X-RAY-DIFFRACTION FOR STUDIES OF SOLID-STATE REACTIONS AND PHASE-TRANSITIONS

被引：1

作者：

JUEZLORENZO, M ^{[1
]}

KOLARIK, V ^{[1
]}

HERRMANN, M ^{[1
]}

ENGEL, W ^{[1
]}

EISENREICH, N ^{[1
]}

机构：

[1] FRAUNHOFER INST CHEM TECHNOL,D-76327 BERGHAUSEN,GERMANY

来源：

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1994年 / 349卷 / 1-3期

关键词：

D O I：

10.1007/BF00323252

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Three examples for the application of time and temperature resolved X-ray diffraction for the investigation of solid state reactions and phase transitions are given. Samples were submitted to an isothermal temperature program or to stepwise heating/cooling, while diffraction patterns were measured continuously. The applications include the in situ identification of reaction products or phases, the determination of kinetic parameters, the observation of thermal expansion and the formation of layers.

引用

页码：163 / 165

页数：3

共 50 条

[31] SOLID-STATE KINETIC MEASUREMENTS USING DYNAMIC X-RAY-DIFFRACTION [J].

ANDERSON, DE ;

THOMSON, WJ .

INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 1987, 26 (08) :1628-1632

[32] THE POLYMER BATTERY AS AN ENVIRONMENT FOR INSITU X-RAY-DIFFRACTION STUDIES OF SOLID-STATE ELECTROCHEMICAL PROCESSES [J].

GUSTAFSSON, T ;

THOMAS, JO ;

KOKSBANG, R ;

FARRINGTON, GC .

ELECTROCHIMICA ACTA, 1992, 37 (09) :1639-1643

[33] X-RAY-DIFFRACTION STUDY OF PHASE-TRANSITIONS IN SODIUM, RUBIDIUM AND POTASSIUM TRIHYDROSELENITE CRYSTALS [J].

AKNAZAROV, SK ;

SHEKHTMA.VS ;

SHUVALOV, LA .

KRISTALLOGRAFIYA, 1974, 19 (06) :1291-1293

[34] X-RAY-DIFFRACTION STUDY OF STRUCTURAL PHASE-TRANSITIONS IN POLYCRYSTALLINE BAPBO3 [J].

ZHUROV, VV ;

IVANOV, SA ;

OLKHOVIK, IV ;

POLITOVA, ED .

KRISTALLOGRAFIYA, 1993, 38 (04) :186-193

[35] X-RAY-DIFFRACTION STUDY OF THE CRYSTAL-STRUCTURES OF HEXAMETHYLETHANE AND ITS PHASE-TRANSITIONS [J].

REYNOLDS, PA .

MOLECULAR PHYSICS, 1979, 37 (05) :1333-1348

[36] LOW-TEMPERATURE X-RAY-DIFFRACTION AND PHASE-TRANSITIONS IN DYVO4 AND DYASO4 [J].

GOBEL, H ;

WILL, G .

PHYSICA STATUS SOLIDI B-BASIC RESEARCH, 1972, 50 (01) :147-&

[37] X-RAY-DIFFRACTION STUDY OF THE STRUCTURE AND PHASE-TRANSITIONS OF C-60-CLATHRATES [J].

TEGZE, M ;

BORTEL, G ;

FAIGEL, G ;

OSZLANYI, G ;

PEKKER, S ;

STEPHENS, PW .

NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1995, 97 (1-4) :585-587

[38] AN X-RAY-DIFFRACTION STUDY OF STRUCTURAL PHASE-TRANSITIONS OF LITHIUM POTASSIUM-SULFATE [J].

CHEN, RH ;

WU, RT .

JOURNAL OF PHYSICS-CONDENSED MATTER, 1989, 1 (39) :6913-6920

[39] Studying solid-state reactions with time-resolved diffraction. [J].

O'Hare, D ;

Walton, R ;

Millange, F ;

Lixu, L .

ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2000, 219 :U774-U774

[40] A UNIQUE HIGH-PRESSURE APPARATUS FOR X-RAY-DIFFRACTION STUDIES OF PHASE-TRANSITIONS UP TO 5 KBAR [J].

HAMAYA, N ;

KUROIWA, Y ;

FUJII, Y .

NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1987, 29 (03) :537-543

← 1 2 3 4 5 →