BETA-PHOSPHORYLATED 5 MEMBERED RING NITROXIDES - SYNTHESIS AND EPR STUDY

被引：29

作者：

DEMBKOWSKI, L ^{[1
]}

FINET, JP ^{[1
]}

FREJAVILLE, C ^{[1
]}

LEMOIGNE, F ^{[1
]}

MAURIN, R ^{[1
]}

MERCIER, A ^{[1
]}

PAGES, P ^{[1
]}

STIPA, P ^{[1
]}

TORDO, P ^{[1
]}

机构：

[1] UNIV AIX MARSEILLE 1,CNRS,URA 1412,RADICAUX LIBRES & SYNTHESE,CASE 521,F-13397 MARSEILLE 4,FRANCE

来源：

FREE RADICAL RESEARCH COMMUNICATIONS | 1993年 / 19卷

关键词：

BETA-PHOSPHORYLATED NITROXIDES; ALPHA-AMINOPHOSPHONATES; INTRAMOLECULAR AMINOMERCURATION; 1-PYRROLINE-N-OXIDES; EPR;

D O I：

10.3109/10715769309056s23

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

A series of stable beta-phosphorylated five membered ring nitroxides was prepared by intramolecular aminomercuration of alkenyl alpha-aminophosphonates. The structure of these nitroxides was deduced from their C-13 and P-31 coupling constants and from force field calculations.

引用

页码：S23 / S32

页数：10

共 24 条

[1] THEORETICAL INTERPRETATION OF THE LINE-SHAPE OBTAINED BY DYNAMIC POLARIZATION IN SOLUTIONS OF FREE-RADICALS [J].

AYANT, Y ;

BESSON, R ;

CASALEGNO, R .

JOURNAL DE PHYSIQUE, 1980, 41 (10) :1183-1192

[2] EFFECT OF RELAXATION PROCESS ON COEFFICIENT OF DYNAMIC POLARIZATION IN SOLUTIONS OF FREE-RADICALS IN LOW FIELDS [J].

AYANT, Y ;

CASALEGNO, R .

JOURNAL DE PHYSIQUE, 1978, 39 (03) :235-245

[3]

AYANT Y, 1990, C AMP MAGN RES REL P, P188

[4]

BERCHADSKY Y, 1990, Patent No. 2225015

[5]

BERLINER LJ, 1976, THEORY APPLICATIONS, V1

[6]

BERLINER LJ, 1979, THEORY APPLICATIONS, V2

[7] KINETIC APPLICATIONS OF ELECTRON PARAMAGNETIC RESONANCE SPECTROSCOPY .3. SELF-REACTIONS OF DIALKYL NITROXIDE RADICALS [J].

BOWMAN, DF ;

GILLAN, T ;

INGOLD, KU .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1971, 93 (24) :6555-&

[8]

CHIGNELL CF, 1984, SPIN LABELLING PHARM, P131

[9]

Janzen E G, 1987, Free Radic Res Commun, V4, P115

[10]

Janzen E. G. T., 1992, BIOACTIVE SPIN LABEL, P573, DOI [10.1007/978-3-642-48724-8_24, DOI 10.1007/978-3-642-48724-8_24]

← 1 2 3 →