3 beta-Acetoxy-19-hydroxy- Delta(5)-pregnen-20-one

被引：0

作者：

zu Greffen, Aike Meier ^{[1
]}

Kranz, Darius P. ^{[1
]}

Neudoerfl, Joerg-M. ^{[1
]}

Schmalz, Hans-Guenther ^{[1
]}

机构：

[1] Univ Cologne, Dept Chem, Greinstr 4, D-50939 Cologne, Germany

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2013年 / 69卷

关键词：

data-to-parameter ratio = 9.9; mean σ(C-C) = 0.003 Å; R factor = 0.037; single-crystal X-ray study; T = 100 K; wR factor = 0.079;

D O I：

10.1107/S1600536813002493

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C23H34O4, the C/D and D/E rings are trans fused and the A/B ring possesses an anti fusion. The two cyclohexane rings adopt a chair conformation while the cyclohexene ring exhibits a half- chair conformation. The cyclopentane ring displays an envelope conformation with the C atom bearing the methyl group as the flap. In the crystal, the molecules are linked by O-H...O hydrogen bonds, forming chains along the b axis.

引用

页码：O313 / +

页数：10

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