Synthesis and characterization of core-shell Fe3O4@collagen nanoparticle, and application as catalyst in green synthesis of benzimidazoles and benzothiazoles

被引:0
作者
Ghafuri, Hossein [1 ]
Esmaili, Elahe [1 ]
Talebi, Majid [1 ]
机构
[1] Iran Univ Sci & Technol, Dept Chem, POB 16846-13114, Tehran, Iran
来源
18TH INTERNATIONAL ELECTRONIC CONFERENCE ON SYNTHETIC ORGANIC CHEMISTRY | 2014年
关键词
Green synthesis; Nanoparticle; Fe3O4@Collagen; benzimidazoles; benzothiazoles;
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Nanoparticles are nanostructures with at least one dimension being less than 100 nm. In this research, nanomagnetic Fe3O4@Collagen was prepared and characterized by Fourier transforms infrared spectroscopy (FT-IR) spectra, Scanning electron microscopy (SEM) images, energy dispersive X-ray spectroscopy (EDX) spectra, X-ray diffraction (XRD) measurements. Fe3O4@collagen is a new and green nano catalysis and using in synthesis of benzimidazoles and benzothiazoles. This method offers several advantages including high yields, short reaction times, easy work up procedure, reusability of catalyst and environmentally benign reaction conditions.
引用
收藏
页数:8
相关论文
共 30 条
[11]   Hydration/hydrolysis by solid acids [J].
Izumi, Y .
CATALYSIS TODAY, 1997, 33 (04) :371-409
[12]   Synthesis of 2-arylbenzimidazoles catalyzed by transition metal nitrates [J].
Kalhor, Mehdi ;
Mobinikhaledi, Akbar ;
Jamshidi, Javad .
RESEARCH ON CHEMICAL INTERMEDIATES, 2013, 39 (07) :3127-3133
[13]  
Kenny R. S., 2006, J HET CHEM, V43, P1376
[14]   Copper-Catalyzed, One-Pot, Three-Component Synthesis of Benzimidazoles by Condensation and C-N Bond Formation [J].
Kim, Yong ;
Kumar, Manian Rajesh ;
Park, Namjin ;
Heo, Yumi ;
Lee, Sunwoo .
JOURNAL OF ORGANIC CHEMISTRY, 2011, 76 (23) :9577-9583
[15]   Solvent-free synthesis of 2-aryl and 2-alkylbenzothiazoles on silica gel under microwave irradiation [J].
Kodomari, M ;
Tamaru, Y ;
Aoyama, T .
SYNTHETIC COMMUNICATIONS, 2004, 34 (16) :3029-3036
[16]   Fast and efficient method for the synthesis of 2-arylbenzimidazoles using MCM-41-SO3H [J].
Mahdavinia, Gholam Hossein ;
Rostamizadeh, Shahnaz ;
Amani, Ali Mohammad ;
Sepehrian, Hamid .
HETEROCYCLIC COMMUNICATIONS, 2012, 18 (01) :33-37
[17]   AN EFFICIENT SYNTHESIS OF 2-ARYLBENZOTHIAZOLES USING SILICA SULFURIC ACID, OXALIC ACID AND ALUMINUM CHLORIDE HYDRATE AS HETEROGENEOUS AND HOMOGENEOUS CATALYST SYSTEMS [J].
Maleki, Behrooz .
COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS, 2011, 76 (01) :27-37
[18]   Advances in the synthesis and catalytic applications of organosulfonic-functionalized mesostructured materials [J].
Melero, Juan A. ;
van Grieken, Rafael ;
Morales, Gabriel .
CHEMICAL REVIEWS, 2006, 106 (09) :3790-3812
[19]   Microwave-assisted one-pot synthesis of benzothiazole and benzoxazole libraries as analgesic agents [J].
Praveen, C. ;
Nandakumar, A. ;
Dheenkumar, P. ;
Muralidharan, D. ;
Perumal, P. T. .
JOURNAL OF CHEMICAL SCIENCES, 2012, 124 (03) :609-624
[20]   Oxidative rearrangement and cyclisation of N-substituted amidines using iodine(III) reagents and the influence of leaving group on mode of reaction [J].
Ramsden, CA ;
Rose, HL .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1997, (16) :2319-2327