A CONVENIENT METHOD FOR THE SYNTHESIS OF DIACYL DISULFIDES

被引：9
|
作者：
WANG, JX
CUI, WF
HU, YL
ZHAO, K
机构：
[1] Institute of Chemistry, Department of Chemistry, Northwest Normal University
来源：
SYNTHETIC COMMUNICATIONS | 1995年 / 25卷 / 06期
关键词：
D O I：
10.1080/00397919508013426
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A simple and general method for the synthesis of diacyl disulfides is reported. Sulfur is allowed to react with sodium hydroxide to give sodium disulfide at 65 degrees C under PTC, which can react with acyl halides to afford diacyl disulfides in good to excellent isolated yields. The effects of solvents and phase transfer catalysts are discussed.
引用
收藏
页码：889 / 898
页数：10
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