4-[(E)-(4-Fluorobenzylidene) amino]-3-methyl-1H-1,2,4-triazole-5(4H)-thione

被引：5

作者：

Devarajegowda, H. C. ^{[1
]}

Jeyaseelan, S. ^{[1
]}

Sathishkumar, R. ^{[2
]}

D'souza, Agnes Sylvia ^{[3
]}

D'souza, Alphonsus ^{[3
]}

机构：

[1] Univ Mysore, Yuvarajas Coll Constituent Coll, Dept Phys, Mysore 570005, Karnataka, India

[2] Indian Inst Sci, Solid State & Struct Chem Unit, Bangalore, Karnataka, India

[3] St Philomenas Coll, Dept Chem, Mysore 570015, Karnataka, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

D O I：

10.1107/S1600536812019174

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the asymmetric unit of the title compound, C10H9FN4S, there are two independent molecules in which the dihedral angles between the 1,2,4-triazole and benzene rings are 36.85 (10) and 7.81 (10)degrees. In the crystal, N-H center dot center dot center dot S interactions link pairs of independent molecules into dimers. There are also pi-pi interactions between the triazole and benzene rings of inversion-related pairs of the more planar molecule [centroid-centroid distance = 3.6430 (13) angstrom].

引用

页码：O1607 / +

页数：8

共 50 条

[1] Crystal structure of 4-[(E)-(4-fluorobenzylidene)amino]-3-methyl-1H-1,2,4-triazole-5(4H)-thione
Manjula, P. S.
Sarojini, B. K.
Narayana, B.
Byrappa, K.
Kumar, S. Madan
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O912 - U510
[2] 4-[(E)-(4-Chlorobenzylidene) amino]-3-methyl-1H-1,2,4-triazole-5(4H)-thione
Sarojini, B. K.
Manjula, P. S.
Kaur, Manpreet
Anderson, Brian J.
Jasinski, Jerry P.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O57 - +
[3] 3-Ethyl-4-[(E)-(4-fluorobenzylidene)amino]-1H-1,2,4-triazole-5(4H)-thione
Jeyaseelan, S.
Devarajegowda, H. C.
Sathishkumar, R.
D'souza, Agnes Sylvia
D'souza, Alphonsus
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1407 - +
[4] 4-[(E)-4-bromobenzylideneamino]-3-methyl-1H-1,2,4-triazole-5(4H)-thione
Fun, Hoong-Kun
Jebas, Samuel Robinson
Sujith, K. V.
Patil, P. S.
Kalluraya, B.
Muralidharan, A.
Dharmaprakash, S. M.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1509 - U2454
[5] 4-[(4-Fluorobenzylidene)amino]-3-[1-(4-isobutylphenyl)ethyl]-1H-1,2,4-triazole-5(4H)-thione
Fun, Hoong-Kun
Loh, Wan-Sin
Vinayaka, A. C.
Kalluraya, B.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O2079 - U1354
[6] The crystal structures of three 3-methyl-1H-1,2,4triazole-5-thiones, including a second polymorph of 4-[(E)-(5-bromo-2-hydroxybenzylidene)amino]-3methyl-1H-1,2,4-triazole-5(4H)-thione and a redetermination of 4-amino-3-methyl-1H-1,2,4-triazole-5(4H)-thione
Manjula, Padmanabha S.
Sarojini, Balladka K.
Yathirajan, Hemmige S.
Akkurt, Mehmet
Ersanli, Cem Cuneyt
Glidewell, Christopher
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : 1003 - +
[7] 3-Methyl-4-{(E)-[4-(methylsulfanyl)-benzylidene]amino}-1H-1,2,4-triazole-5(4H)-thione
Sarojini, B. K.
Manjula, P. S.
Hegde, Gurumurthy
Kour, Dalbir
Gupta, Vivek K.
Kant, Rajni
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O718 - +
[8] 4-[(E)-(4-Hydroxybenzylidene)amino]-3- methyl-1H-1,2,4-triazole-5(4H)-thione
Sarojini, Balladka K.
Manjula, Padmanabha S.
Narayana, B.
Jasinski, Jerry P.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O733 - +
[9] (E)-4-[(4-Fluorobenzylidene)amino]-3-[1-(4-isobutylphenyl)ethyl]-1-(morpholinomethyl)-1H-1,2,4-triazole-5(4H)-thione methanol hemisolvate
Goh, Jia Hao
Fun, Hoong-Kun
Vinayaka, A. C.
Kalluraya, B.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1233 - U1390
[10] 4-(5-Bromo-2-hydroxybenzylidene-amino)-3-methyl-1H-1,2,4-triazole-5-(4H)-thione
Wang, Min
Cao, Minna
Hu, Bo
Cheng, CuiXia
Song, XueGang
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O374 - U1739

← 1 2 3 4 5 →