3,5-BIS(TRIFLUOROMETHYL)PYRAZOLE AND SOME N-SUBSTITUTED DERIVATIVES

被引：41
|
作者：
CLAIRE, PPK
COE, PL
JONES, CJ
MCCLEVERTY, JA
机构：
[1] School of Chemistry, University of Birmingham, Birmingham, B15 2TT
来源：
JOURNAL OF FLUORINE CHEMISTRY | 1991年 / 51卷 / 02期
关键词：
D O I：
10.1016/S0022-1139(00)80298-5
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The pyrazoles [CF3]2C3HN2R [R = H, COPh, C6F5, C6H4NO2-4 and C6H3[NO2]2-2,4] have been prepared in yields ranging from 27% [R = C6F5] to 78% [R = C6H3[NO2]2-2,4] by the reaction between 1,1,1,5,5,5-hexafluoropentane-2,4-dione and the appropriately substituted hydrazine, NH2NHR.
引用
收藏
页码：283 / 289
页数：7
相关论文
共 50 条
  • [1] CARBONYLRHODIUM(I) DERIVATIVES OF 3,5-DIMETHYL AND 3,5-BIS(TRIFLUOROMETHYL)PYRAZOLE
    BANDITELLI, G
    BANDINI, AL
    BONATI, F
    MINGHETTI, G
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1981, 218 (02) : 229 - 239
  • [2] POSITIVE AND NEGATIVE-ION MASS-SPECTROMETRY OF CARBONYLRHODIUM(I) DERIVATIVES OF 3,5-DIMETHYL(TRIFLUOROMETHYL)PYRAZOLE AND 3,5-BIS(TRIFLUOROMETHYL)PYRAZOLE
    TRALDI, P
    VETTORI, U
    BANDITELLI, G
    BANDINI, AL
    MINGHETTI, G
    INORGANICA CHIMICA ACTA-ARTICLES, 1983, 69 (FEB): : 207 - 214
  • [3] Synthesis of 3,5-Bis(trifluoromethyl)phenyl-Substituted Pyrazole Derivatives as Potent Growth Inhibitors of Drug-Resistant Bacteria
    Alkhaibari, Ibrahim S.
    Kc, Hansa Raj
    Roy, Subrata
    Abu-gazleh, Mohd. K.
    Gilmore, David F.
    Alam, Mohammad A.
    MOLECULES, 2021, 26 (16):
  • [4] The structure of 3,5-bis(trifluoromethyl)pyrazole in the gas phase and in the solid state
    Alkorta, I
    Elguero, J
    Donnadieu, B
    Etienne, M
    Jaffart, J
    Schagen, D
    Limbach, HH
    NEW JOURNAL OF CHEMISTRY, 1999, 23 (12) : 1231 - 1237
  • [5] Exploring Arylazo-3,5-Bis(trifluoromethyl)pyrazole Switches
    Enache, Bogdan C.
    Hanganu, Anamaria
    Tablet, Cristina
    Anghel, Catalin C.
    Popescu, Codruta C.
    Paun, Anca
    Hadade, Niculina Daniela
    Madalan, Augustin M.
    Matache, Mihaela
    ACS OMEGA, 2022, : 39122 - 39135
  • [6] N-[3,5-Bis(trifluoromethyl)phenyl]salicylaldimine
    Karadayi, N
    Gözüyesil, S
    Güzel, B
    Büyükgüngör, O
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O161 - O163
  • [7] Dimethylammonium 3,5-bis(trifluoromethyl)pyrazolide
    Vitze, Hannes
    Lerner, Hans-Wolfram
    Bolte, Michael
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O3462 - U3051
  • [8] A PRACTICAL AND SAFE PREPARATION OF 3,5-BIS(TRIFLUOROMETHYL)ACETOPHENONE (1-[3,5-Bis(trifluoromethyl) phenyl]-ethanone)
    Leazer, Johnnie L., Jr.
    Cvetovich, Raymond
    ORGANIC SYNTHESES, 2005, 82 : 115 - +
  • [9] Synthesis and Evaluation of Anti-inflammatory N-Substituted 3,5-Bis(2-(trifluoromethyl)benzylidene)piperidin-4-ones
    Xie, Zixin
    Zhang, Zaikui
    Yu, Shufang
    Cheng, Donghua
    Zhang, Huan
    Han, Chao
    Lv, Handeng
    Ye, Faqing
    CHEMMEDCHEM, 2017, 12 (04) : 327 - 336
  • [10] N-[3,5-bis(trifluoromethyl)phenyl]-3-methoxysalicylaldimine
    Karadayi, N
    Gözüyesil, S
    Güzel, B
    Büyükgüngör, O
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O851 - O853
12345