DETERMINATION OF SYNEPHRINE IN ORIENTAL PHARMACEUTICAL DECOCTIONS CONTAINING AURANTII NOBILIS PERICARPIUM BY ION-PAIR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY .2.

被引：2
|
作者：
HASHIMOTO, K [1 ]
UCHIMURA, H [1 ]
SEKI, Y [1 ]
WATANABE, M [1 ]
YASUDA, T [1 ]
OHSAWA, K [1 ]
机构：
[1] TOHOKU COLL PHARMACEUT SCI, 4-1 KOMATSUSHIMA 4 CHOME, AOBA KU, SENDAI, MIYAGI 981, JAPAN
来源：
YAKUGAKU ZASSHI-JOURNAL OF THE PHARMACEUTICAL SOCIETY OF JAPAN | 1993年 / 113卷 / 08期
关键词：
SYNEPHRINE; AURANTII-NOBILIS-PERICARPIUM; ION-PAIR HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY; ORIENTAL PHARMACEUTICAL DECOCTION; QUANTITATIVE DETERMINATION;
D O I：
10.1248/yakushi1947.113.8_600
中图分类号：
R9 [药学];
学科分类号：
1007 ;
摘要：
A simple method using ion-pair high-Performance liquid chromatography was established for the rapid and precise determination of synephrine in thirtythree species of oriental pharmaceutical decoctions containing Aurantii Nobilis Pericarpium. An ODS column and a mixed solvent system of water, acetonitrile, sodium dodecyl sulfate and phosphoric acid as a mobile phase were used for the separation. Synephrine was eluted without interference of other coexisting components within 15 min.
引用
收藏
页码：600 / 603
页数：4
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