DETERMINATION OF ORTHOCHLOROPHENOL BY STRIPPING VOLTAMMETRY

被引:6
作者
MANISANKAR, P [1 ]
PRABU, HG [1 ]
机构
[1] ALAGAPPA UNIV,DEPT IND CHEM,KARAIKKUDI,TAMIL NADU,INDIA
关键词
ORTHOCHLOROPHENOL; GLASSY CARBON; STRIPPING VOLTAMMETRY;
D O I
10.1002/elan.1140070618
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The present work reports on a differential pulse and square wave stripping voltammetric procedure for the determination of orthochlorophenol. The best conditions included using 0.1 MKOH solution, an accumulation potential of 0.4V vs. Ag/AgCl electrode, a square wave amplitude of 60 mV, a frequency of 50Hz, a step potential of 4mV, and an initial scan potential of -1.0V. Under these conditions, determination limits of ng/ml were achieved at a stationary glassy carbon electrode.
引用
收藏
页码:594 / 597
页数:4
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