CRYSTAL-STRUCTURE OF SODIUM 4-AMINOCINNOLINE-3-CARBOXYLATE TETRAHYDRATE

被引：0

作者：

GLOWKA, ML ^{[1
]}

OLCZAK, A ^{[1
]}

STANCZAK, A ^{[1
]}

机构：

[1] MED ACAD LODZ,DEPT PHARMACEUT CHEM & DRUG ANAL,PL-90145 LODZ,POLAND

来源：

POLISH JOURNAL OF CHEMISTRY | 1994年 / 68卷 / 08期

关键词：

X-RAY STRUCTURE; CINNOLINE; SODIUM SALT;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Crystal structure of the title compound has been determined by X-ray method to the final R factor of 0.058 and compared in detail with similar structures from Cambridge Structural Database. It is composed of flat 4-aminocinnoline-3-carboxylate anions and disodium decahydrate dications domains expanded in [010] direction and joint by a complicated system of hydrogen bonds. A strong intramolecular hydrogen bond between amine and carboxy groups roughly maintains coplanarity of the groups with aromatic cinnoline system.

引用

页码：1631 / 1637

页数：7

共 17 条

[1] THE DEVELOPMENT OF VERSION-3 AND VERSION-4 OF THE CAMBRIDGE STRUCTURAL DATABASE SYSTEM
ALLEN, FH
DAVIES, JE
GALLOY, JJ
JOHNSON, O
KENNARD, O
MACRAE, CF
MITCHELL, EM
MITCHELL, GF
SMITH, JM
WATSON, DG
[J]. JOURNAL OF CHEMICAL INFORMATION AND COMPUTER SCIENCES, 1991, 31 (02): : 187 - 204
[2] ANTHRANILIC ACID-I, C7H7NO2, BY NEUTRON-DIFFRACTION
BROWN, CJ
EHRENBERG, M
[J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1985, 41 (MAR) : 441 - 443
[3] STRUCTURAL STUDIES OF ANALGESICS AND THEIR INTERACTIONS .11. CRYSTAL-STRUCTURES OF 1-1 COMPLEXES OF MECLOFENAMIC ACID WITH CHOLINE AND ETHANOLAMINE
DHANARAJ, V
VIJAYAN, M
[J]. BIOCHIMICA ET BIOPHYSICA ACTA, 1987, 924 (01) : 135 - 146
[4] GLOWKA M, 1994, IN PRESS ACTA CRYST, V50
[5] STRUCTURE OF ETHYL 4-OXO-1,2,3,4-TETRAHYDROCINNOLINE-2-ACETATE
GLOWKA, ML
IWANICKA, I
STANCZAK, A
[J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1991, 47 : 668 - 670
[6] STRUCTURES OF 8-CHLORO-1,2,3,4-TETRAHYDROCINNOLIN-4-ONE AND ITS 2-CHLOROACETYL DERIVATIVE
GLOWKA, ML
IWANICKA, I
[J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1991, 47 : 196 - 198
[7] STRUCTURAL INVESTIGATIONS OF BENZO[C]CINNOLINE DERIVATIVES .2. STRUCTURES OF 2-PYRROLIDINOBENZO[C]CINNOLINE AND 4-PYRROLIDINOBENZO[C]CINNOLINE
HOKELEK, T
KILIC, E
TUZUN, C
[J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1991, 47 : 373 - 376
[8] STRUCTURAL INVESTIGATIONS OF BENZO[C]CINNOLINE DERIVATIVES .1. STRUCTURES OF 1-PIPERIDINOBENZO[C]CINNOLINE AND 3-PIPERIDINOBENZO[C]CINNOLINE
HOKELEK, T
KILIC, E
TUZUN, C
[J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1991, 47 : 369 - 373
[9] STRUCTURAL INVESTIGATIONS OF BENZO[C]CINNOLINE DERIVATIVES .3. STRUCTURE OF 2-FLUOROBENZO[C]CINNOLINE
HOKELEK, T
[J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1991, 47 : 1432 - 1434
[10] STRUCTURE OF 1-MORPHOLINOBENZO[C]CINNOLINE
HOKELEK, T
WATKIN, DJ
KILIC, E
TUZUN, C
[J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1990, 46 : 1027 - 1029

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