USE OF DIMETHYLFORMAMIDE SULFUR-TRIOXIDE COMPLEX AS A SULFATING AGENT OF TYROSINE

被引：27

作者：

FUTAKI, S ^{[1
]}

TAIKE, T ^{[1
]}

YAGAMI, T ^{[1
]}

OGAWA, T ^{[1
]}

AKITA, T ^{[1
]}

KITAGAWA, K ^{[1
]}

机构：

[1] UNIV TOKUSHIMA,FAC PHARMACEUT SCI,TOKUSHIMA 770,JAPAN

来源：

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1 | 1990年 / 06期

关键词：

D O I：

10.1039/p19900001739

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Dimethylformamide-sulphur trioxide (DMF-SO3) complex was found to be more suitable for tyrosine sulphation than pyridine-sulphur trioxide (Pyr-SO3) complex, the most commonly used sulphur trioxide complex for sulphation. The work-up after sulphation using DMF-SO3 was also easier than with Pyr-SO3. The usefulness of DMF-SO3 complex was demonstrated through the synthesis of two tyrosine sulphate [Tyr(SO3H)]-containing peptides, leucine-enkephalin sulphate and leucosulfakinin-II.

引用

页码：1739 / 1744

页数：6

共 31 条

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