DETECTION OF ADULTERANTS BY FTIR AND GC-MS IN HERBAL SLIMMING FOOD SUPPLEMENTS

被引:0
|
作者
Popescu, Anca Mihaela [1 ,2 ]
Radu, Gabriel Lucian [2 ]
机构
[1] Natl Res & Dev Inst Food Bioresources, IBA Bucharest, Bucharest, Romania
[2] Univ Politehn Bucuresti, Fac Appl Chem & Mat Sci, Bucharest, Romania
来源
UNIVERSITY POLITEHNICA OF BUCHAREST SCIENTIFIC BULLETIN SERIES B-CHEMISTRY AND MATERIALS SCIENCE | 2015年 / 77卷 / 04期
关键词
Fourier Transform Infrared spectroscopy; gas chromatography-mass spectrometry; adulteration; herbal food supplements; body weight; sibutramine; fluoxetine;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The main objective of this study was to detect the active pharmaceutical ingredients in herbal food supplements designed to reduce body weight using two analytical methods: Fourier Transform Infrared spectroscopy, and gas chromatography coupled with mass spectrometry. 10 dietary supplements were analyzed for the first time in Romania. Three of these food supplements were found to be adulterated with illegal substances such as sibutramine, and fluoxetine.
引用
收藏
页码:221 / 230
页数:10
相关论文
共 50 条
  • [21] Wine markers in archeological potteries: detection by GC-MS at ultratrace levels
    Blanco-Zubiaguirre, Laura
    Olivares, Maitane
    Castro, Kepa
    Antonio Carrero, Jose
    Garcia-Benito, Carlos
    Angel Garcia-Serrano, Jose
    Perez-Perez, Julian
    Perez-Arantegui, Josefina
    ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2019, 411 (25) : 6711 - 6722
  • [22] Wine markers in archeological potteries: detection by GC-MS at ultratrace levels
    Laura Blanco-Zubiaguirre
    Maitane Olivares
    Kepa Castro
    Jose Antonio Carrero
    Carlos García-Benito
    José Ángel García-Serrano
    Julián Pérez-Pérez
    Josefina Pérez-Arantegui
    Analytical and Bioanalytical Chemistry, 2019, 411 : 6711 - 6722
  • [23] ESSENTIAL OIL CHARACTERIZATION IN CLOVE (Syzigium aromaticum Linn.) BY GC-MS AND DETECTION OF ITS ADULTERATION BY ATR- FTIR METHOD
    Ahamad, Javed
    Omer, Alaa Younis
    Khidr, Tara Maghded
    Jameel, Sara Yousif
    APPLIED BIOLOGICAL RESEARCH, 2022, 24 (03) : 309 - 316
  • [24] Comparative analysis of clary sage (S-sclarea L.) oil volatiles by GC-FTIR and GC-MS
    Cai, Jibao
    Lin, Ping
    Zhu, Xiaolan
    Su, Qingde
    FOOD CHEMISTRY, 2006, 99 (02) : 401 - 407
  • [25] Improvement of a GC-MS analytical method for the simultaneous detection of 3-MCPD and 1,3-DCP in food
    Yang, Sehee
    Kwon, Kisung
    Choi, Jangduck
    Jo, Cheon-Ho
    FOOD SCIENCE AND BIOTECHNOLOGY, 2018, 27 (03) : 859 - 866
  • [26] Chemical characterisation of spray paints by a multi-analytical (Py/GC-MS, FTIR, μ-Raman) approach
    Germinario, Giulia
    van der Werf, Inez Dorothe
    Sabbatini, Luigia
    MICROCHEMICAL JOURNAL, 2016, 124 : 929 - 939
  • [27] Characterization of a late bronze age "Kohl Box" from the Cilician Plain using FTIR and GC-MS
    Tarhan, Ismail
    Sahin, Fatma
    JOURNAL OF ARCHAEOLOGICAL SCIENCE-REPORTS, 2023, 50
  • [28] Rapid sample preparation method for LC-MS/MS or GC-MS analysis of acrylamide in various food matrices
    Mastovska, Katerina
    Lehotay, Steven J.
    JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2006, 54 (19) : 7001 - 7008
  • [29] Detection, identification and quantification by 1H NMR of adulterants in 150 herbal dietary supplements marketed for improving sexual performance
    Gilard, Veronique
    Balayssac, Stephane
    Tinaugus, Aurelie
    Martins, Nathalie
    Martino, Robert
    Malet-Martino, Myriam
    JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2015, 102 : 476 - 493
  • [30] Comparison of GC-MS and HPLC for overcoming matrix interferences in the analysis of PAHs in smoked food
    Chiu, CP
    Lin, YS
    Chen, BH
    CHROMATOGRAPHIA, 1997, 44 (9-10) : 497 - 504