Preparation of Needle like Aragonite Precipitated Calcium Carbonate (PCC) from Dolomite by Carbonation Method

被引:16
作者
Ramakrishna, Chilakala [1 ]
Thenepalli, Thriveni [2 ]
Huh, Jae-Hoon [1 ]
Ahn, Ji Whan [2 ]
机构
[1] Hanil Cement Corp, Dept R&D Team, Danyang 27003, South Korea
[2] Korea Inst Geosci & Mineral Resources, Mineral Proc Div, Daejeon 34132, South Korea
关键词
Precipitated calcium carbonate (PCC); Carbonation; Dolomite; Aspect ratio;
D O I
10.4191/kcers.2016.53.1.7
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In this paper, we have developed a simple, new and economical carbonation method to synthesize a pure form of aragonite needles using dolomite raw materials. The obtained aragonite Precipitated Calcium Carbonate (PCC) was characterized by XRD and SEM, for the measurement of morphology, particle size, and aspect ratio (ratio of length to diameter of the particles). The synthesis of aragonite PCC involves two steps. At first, after calcinated dolomite fine powder was dissolved in water for hydration, the hydrated solution was mixed with aqueous solution of magnesium chloride at 80 degrees C, and then CO2 was bubbled into the suspension for 3 h to produce aragonite PCC. Finally, aragonite type precipitated calcium carbonate can be synthesized from natural dolomite via a simple carbonation process, yielding product with average particle size of 30-40 mu m.
引用
收藏
页码:7 / 12
页数:6
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