2-Amino-3-carboxypyridinium chloride hemihydrate

被引：4

作者：

Bouchene, Rafika ^{[1
,2
]}

Bouacida, Sofiane ^{[1
,3
]}

Berrah, Fadila ^{[1
,2
]}

Daran, Jean-Claude ^{[4
]}

机构：

[1] Univ Oum El Bouaghi, LCATM, Oum El Bouaghi, Algeria

[2] Univ Oum El Bouaghi, Fac Sci Exactes & Sci Nat & Vie, Dept Sci Mat, Oum El Bouaghi, Algeria

[3] Univ Mentouri Constantine, Unite Rech Chim Environm & Mol Struct CI IEMS, Constantine, Algeria

[4] UPR CNRS 8241, Lab Chim Coodinat, F-31077 Toulouse 04, France

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

D O I：

10.1107/S1600536812017230

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The asymmetric unit of the title compound, C6H7N2O2+center dot-Cl-center dot 0.5H(2)O, consists of two protonated 2-amino-3-carboxypyridine cations, two chloride anions and one molecule of water. The crystal packing can be described as alternating layers of cations and anions parallel to (110), which are linked together by O-w-H center dot center dot center dot Cl interactions. In the crystal, four types of classical hydrogen bonds are observed, viz. cation-anion (O-H center dot center dot center dot Cl and N-H center dot center dot center dot Cl), cation-cation (N-H center dot center dot center dot O), cation-water (N-H center dot center dot center dot O-w) and water-anion (O-w-H center dot center dot center dot Cl), resulting in the formation of an infinite three-dimensional network.

引用

页码：O1493 / +

页数：9

共 17 条

[1] 2-amino-3-carboxypyridinium dihydrogen phosphate [J].

Akriche, Samah ;

Rzaigui, Mohamed .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 :O3460-U3034

[2]

[Anonymous], 2011, CRYSALIS PRO

[3] Phase transition of pyridinium tetrachloroiodate(III), PyHICl4, studied by a single crystal X-ray analysis and dielectric and heat capacity measurements [J].

Asaji, Tetsuo ;

Eda, Kazuo ;

Fujimori, Hiroki ;

Adachi, Toshinobu ;

Shibusawa, Takayoshi ;

Oguni, Masaharu .

JOURNAL OF MOLECULAR STRUCTURE, 2007, 826 (01) :24-28

[4] Open-framework coordination complexes from hydrogen-bonded networks: toward host/guest complexes [J].

Beatty, AM .

COORDINATION CHEMISTRY REVIEWS, 2003, 246 (1-2) :131-143

[5] 2-Amino-3-carboxypyridinium nitrate [J].

Berrah, Fadila ;

Bouacida, Sofiane ;

Roisnel, Thierry .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O2057-U709

[6] Bis(2-amino-3-carboxypyridinium) sulfate trihydrate [J].

Berrah, Fadila ;

Ouakkaf, Amira ;

Bouacida, Sofiane ;

Roisnel, Thierry .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O953-U1219

[7] 2-Amino-3-carboxypyrazin-1-ium nitrate monohydrate [J].

Berrah, Fadila ;

Ouakkaf, Amira ;

Bouacida, Sofiane ;

Roisnel, Thierry .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O525-U2056

[8]

Bouacida S., 2008, THESIS

[9]

Brandenburg K, 2001, DIAMOND

[10] SIR2004:: an improved tool for crystal structure determination and refinement [J].

Burla, MC ;

Caliandro, R ;

Camalli, M ;

Carrozzini, B ;

Cascarano, GL ;

De Caro, L ;

Giacovazzo, C ;

Polidori, G ;

Spagna, R .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2005, 38 :381-388

← 1 2 →