PORE-SIZE DISTRIBUTION IN SEPARON USING MERCURY CONTACT ANGLES IN PORES AND HYSTERESIS IN POROSIMETRY

被引:5
作者
KLOUBEK, J [1 ]
机构
[1] CZECHOSLOVAK ACAD SCI,J HEYROVSKY INST PHYS CHEM & ELECTROCHEM,CS-18223 PRAGUE 8,CZECHOSLOVAKIA
关键词
CONTACT ANGLE HYSTERESIS; CONTACT ANGLE OF MERCURY IN PORES; HYSTERESIS IN POROSIMETRY; MERCURY POROSIMETRY; PORE POTENTIAL; PORE STRUCTURE; SORBENT FOR HPLC;
D O I
10.1163/156856192X01033
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
The porous co-polymer Separon HEMA 1000 for HPLC column packing was examined by using a special method of mercury porosimetry evaluation. The advancing and receding contact angles of mercury in pores were determined and the method used is described in detail. The pore distribution curves obtained from mercury porosimetry and from the nitrogen desorption isotherms are in good agreement. The dependence of the hysteresis of the porosimetry curves and mercury retention in the pores on the intrusion volume was investigated to characterize the porous structure of the sample. The influence of the pore potential on the hysteresis was evaluated.
引用
收藏
页码:667 / 688
页数:22
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