SOME NOVEL LEAD(IV) TETRACARBOXYLATES - REAGENTS FOR CARBON-CARBON BOND FORMATION

被引：0

作者：

MOLONEY, MG

PAUL, DR

THOMPSON, RM

机构：

[1] UNIV OXFORD,DYSON PERRINS LAB,OXFORD OX1 3QY,ENGLAND

[2] ASSOCIATED OCTEL CO,WIRRAL L65 4HF,ENGLAND

来源：

MAIN GROUP METAL CHEMISTRY | 1995年 / 18卷 / 06期

关键词：

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The preparation of a range of lead(IV) complexes by metathesis of lead tetraacetate with di- and tri-carboxylic acids is described, and these compounds have been characterised by a combination of H-1, C-13 and Pb-207 NMR spectroscopy. Some of these compounds represent the first complexes of lead(IV) to have been prepared from podal ligands. These complexes can be used for the alpha-arylation of beta-dicarbonyl substrates, in comparable yield to that achieved with lead tetraacetate.

引用

页码：295 / 298

页数：4

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