Three new phenolic glucosides were isolated from the leaves of Osmanthus asiaticus NAKAI (Oleaceae). The structures of 1, 2 and 3 were determined to be 2-hydroxy-5-(2-hydroxyethyl)phenyl beta-D-glucopyranoside, 4-(2,3-dihydroxypropyl)-2,6-dimethoxyphenyl beta-D-glucopyranoside and D-threo-guaiacylglycerol 7-O-beta-D-glucopyranoside, respectively, on the basis of chemical and spectral data.