COMPLETE ASSIGNMENT OF THE H-1 AND C-13 NMR-SPECTRA OF A PENTACYCLO [5.4.0.0(2,6).0(3,10).0(5,9)]UNDECANE DERIVATIVE

被引：21

作者：

CADD, DH ^{[1
]}

FEAST, WJ ^{[1
]}

KENWRIGHT, AM ^{[1
]}

SAY, JM ^{[1
]}

机构：

[1] UNIV DURHAM,INTERDISCIPLINARY RES CTR POLYMER SCI & TECHNOL,SOUTH RD,DURHAM DH1 3LE,ENGLAND

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 1993年 / 31卷 / 09期

关键词：

H-1; NMR; C-13; TRICYCLIC UNDECANE DERIVATIVES; PENTACYCLIC UNDECANE DERIVATIVES;

D O I：

10.1002/mrc.1260310903

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The production of compounds derived from intramolecular photocycloaddition reactions upon Diels-Alder adducts has received considerable attention, but assignment of the NMR spectra of the photoaddition products has proved problematic, rendering structural determination difficult. This paper reports the complete assignments of the proton and carbon NMR spectra of 11,11-dimethoxypentacyclo[5.4.0.0(2,6).0(3,10).0(5,9)]undecan-8-one and the assignment of the spectra of pentacyclo [5.4.0.0(2,6).0(3,10).0(5,9)]undecan-8,11-dione by analogy.

引用

页码：801 / 807

页数：7

共 29 条

[21]

NOBEL A, 1863, Patent No. 2359

[22] SELECTIVE POPULATION INVERSION (SPI) - PULSED DOUBLE-RESONANCE METHOD IN FT NMR-SPECTROSCOPY EQUIVALENT TO INDOR [J].

PACHLER, KGR ;

WESSELS, PL .

JOURNAL OF MAGNETIC RESONANCE, 1973, 12 (03) :337-339

[23] C-13-H-1 SHIFT CORRELATION WITH FULL H-1-H-1 DECOUPLING [J].

PERPICKDUMONT, M ;

REYNOLDS, WF ;

ENRIQUEZ, RG .

MAGNETIC RESONANCE IN CHEMISTRY, 1988, 26 (05) :358-361

[24] MULTIPLE QUANTUM FILTERS FOR ELUCIDATING NMR COUPLING NETWORKS [J].

PIANTINI, U ;

SORENSEN, OW ;

ERNST, RR .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1982, 104 (24) :6800-6801

[25] IMPROVED C-13-H-1 SHIFT CORRELATION SPECTRA FOR INDIRECTLY BONDED CARBONS AND HYDROGENS - THE FLOCK SEQUENCE [J].

REYNOLDS, WF ;

MCLEAN, S ;

PERPICKDUMONT, M ;

ENRIQUEZ, RG .

MAGNETIC RESONANCE IN CHEMISTRY, 1989, 27 (02) :162-169

[26] C-13 - H-1 SHIFT CORRELATION WITH FULL H-1 - H-1 DECOUPLING .2. FURTHER SIGNIFICANT IMPROVEMENTS IN RESOLUTION AND SENSITIVITY [J].

REYNOLDS, WF ;

MCLEAN, S ;

PERPICKDUMONT, M ;

ENRIQUEZ, RG .

MAGNETIC RESONANCE IN CHEMISTRY, 1988, 26 (12) :1068-1074

[27]

Sax N.I., 1986, SAXS DANGEROUS PROPE, P54

[28] SUPPRESSION OF J-CROSS-TALK IN SUBSPECTRAL EDITING - THE SEMUT GL PULSE SEQUENCE [J].

SORENSEN, OW ;

DONSTRUP, S ;

BILDSOE, H ;

JAKOBSEN, HJ .

JOURNAL OF MAGNETIC RESONANCE, 1983, 55 (02) :347-354

[29] THE 1-1 AND 2-1 ADDUCTS OF CYCLOPENTADIENE WITH PARA-BENZOQUINONE [J].

YATES, P ;

SWITLAK, K .

CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 1990, 68 (10) :1894-1900

← 1 2 3 →