PREPARATION OF ACTIVE ZINC BY REDUCTION OF ZINC-CHLORIDE WITH SODIUM IN LIQUID-AMMONIA AND ITS USE IN THE BARBIER REACTION

被引：7

作者：

MAKOSZA, M

GRELA, K

机构：

[1] Institute of Organic Chemistry, Polish Academy of Sciences, Kasprzaka 44

来源：

TETRAHEDRON LETTERS | 1995年 / 36卷 / 50期

关键词：

D O I：

10.1016/0040-4039(95)01948-H

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Active dnc ponder produced by reduction of anhydrous dnc chloride with solution of sodium in liquid ammonia exhibits high reactivity in the Barbier type reaction both in THF and liquid ammonia solution.

引用

页码：9225 / 9226

页数：2

共 18 条

[1] Preparation of active zinc by reduction of zinc chloride with sodium in liquid ammonia and its use in the Barbier reaction
Makosza, M.
Grela, K.
Tetrahedron Letters, 36 (50):
[2] ON THE DIFFERENCE IN THE RESULTS OF REDUCTIVE DEFLUORINATION OF PENTAFLUOROBENZOIC ACID BY SODIUM AND ZINC IN LIQUID-AMMONIA MEDIUM
LAEV, SS
SHTEINGARTS, VD
BILKIS, II
TETRAHEDRON LETTERS, 1995, 36 (26) : 4655 - 4658
[3] SOLUBILITY OF CARBON-DIOXIDE IN LIQUID SOLUTIONS OF ZINC-CHLORIDE IN SODIUM-CHLORIDE AND IN POTASSIUM-CHLORIDE
SOKOLOWSKI, A
BORODZINSKI, A
JOURNAL OF CHEMICAL THERMODYNAMICS, 1979, 11 (05): : 421 - 427
[4] ZINC-PROMOTED REDUCTIVE COUPLING REACTIONS - REACTION OF SODIUM METHOXYALKENYLDIALKYLBORATES(1-) WITH ALKENYLZINC CHLORIDES OR ZINC-CHLORIDE
MOLANDER, GA
ZINKE, PW
ORGANOMETALLICS, 1986, 5 (10) : 2161 - 2162
[5] A NEW REDUCTION OF SOME CARBOXYLIC ESTERS WITH SODIUM-BOROHYDRIDE AND ZINC-CHLORIDE IN THE PRESENCE OF A TERTIARY AMINE
YAMAKAWA, T
MASAKI, M
NOHIRA, H
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1991, 64 (09) : 2730 - 2734
[6] ZINC-CHLORIDE AND ITS SOLUTIONS IN POLYETHYLENEGLYCOL ARE NEW STEADY LIQUID-PHASES IN GAS-CHROMATOGRAPHY
STAROBINETS, GL
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VINARSKY, VA
ZHITKEVICH, NV
DOKLADY AKADEMII NAUK BELARUSI, 1989, 33 (09): : 819 - 822
[7] A CONVENIENT METHOD FOR THE PREPARATION OF SECONDARY PROPARGYLIC ETHERS - THE REACTION OF ACETALS WITH 1-TRIMETHYLSILYLALKYNES PROMOTED BY THE COMBINED USE OF CATALYTIC AMOUNTS OF TIN(IV) CHLORIDE AND ZINC-CHLORIDE
HAYASHI, M
INUBUSHI, A
MUKAIYAMA, T
CHEMISTRY LETTERS, 1987, (10) : 1975 - 1978
[8] Convenient preparation of 'high-surface sodium' in liquid ammonia: Use in the acyloin reaction
Makosza, M
Grela, K
SYNLETT, 1997, (03) : 267 - +
[9] AN ANOMALOUS OPENING OF A THIOPHENE RING UPON THE REDUCTION OF THIOPHENE-2-CARBOXYLIC ACID BY SODIUM IN LIQUID-AMMONIA CATALYZED BY FERRIC-CHLORIDE
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GOLDFARB, YL
STOYANOVICH, FM
BULLETIN OF THE ACADEMY OF SCIENCES OF THE USSR DIVISION OF CHEMICAL SCIENCE, 1985, 34 (03): : 661 - 661
[10] A CONVENIENT METHOD FOR THE PREPARATION OF SECONDARY PROPARGYLIC ETHERS - THE REACTIONS OF ACETALS WITH 1-TRIMETHYLSILYL-1-ALKYNES PROMOTED BY THE COMBINED USE OF CATALYTIC AMOUNTS OF TIN(IV) CHLORIDE AND ZINC-CHLORIDE
HAYASHI, M
INUBUSHI, A
MUKAIYAMA, T
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1988, 61 (11) : 4037 - 4042

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