DETERMINATION OF ORGANIC COMPOUNDS IN WATER USING INHIBITORY EFFECT ON THE LUMINOL-HYDROGEN PEROXIDE-PEROXODISULFATE CHEMILUMINESCENCE REACTION

被引：2
|
作者：
Sato, Kenji [1 ]
Tanaka, Shigeyuki [1 ]
机构：
[1] Iwaki Meisei Univ, Coll Sci & Engn, Dept Fundamental Sci, Iwaki, Fukushima 970, Japan
来源：
ANALYTICAL SCIENCES | 1991年 / 7卷
关键词：
geosmin; 2-methylisoborneol; luminol; chemiluminescence; environmental analysis;
D O I：
10.2116/analsci.7.Supple_1167
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A simple and rapid method for the determination of such organic compounds as geosmin, 2-methylisoborneol(2-MIB) was investigated by chemiluminescence method. Luminol-hydrogen peroxidepotassium peroxodisulfate co-oxidation system in alkaline solution was adopted as chemiluminescence reaction. The chemiluminescence intensity was clearly decreased with an increase in concentration of geosmin and 2-MIB. The concentrations of geosmin and 2-MIB were measured by using the inhibitory effect on the CL,"reaction. The detection limits for these compounds were 5.5x100(-11) M for geosmin and 1.2x10(-11) M for 2-MIB. The relative standard deviations(n=5) for 15.5x10(-11) geosmin and 1.2x10(-10) M 2-MIB were 5.4% and 10%, respectively.
引用
收藏
页码：1167 / 1170
页数：4
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