rac-3-[(Anilino)(naphthalen-2-yl)methyl]-thian-4-one

被引：2

作者：

Harms, Klaus ^{[1
]}

Abaee, M. Saeed ^{[2
]}

Mojtahedi, Mohammad M. ^{[2
]}

Mesbah, A. Wahid ^{[2
]}

机构：

[1] Philipps Univ Marburg, Fachbereich Chem, Hans Meerwein Str, D-35032 Marburg, Germany

[2] Chem & Chem Engn Res Ctr Iran, Dept Organ Chem, Tehran, Iran

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

data-to-parameter ratio = 14.1; mean σ(C-C) = 0.003 Å; R factor = 0.033; single-crystal X-ray study; T = 193 K; wR factor = 0.074;

D O I：

10.1107/S1600536812005983

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C 22H 21NOS, the thio-pyran-one ring adopts a chair-like conformation with the substituent in the axial position. The relative configuration of the racemic compound is 3R,7S according to the numbering scheme used in this publication. In the crystal packing, centrosymmetric dimers are built up via N - H⋯O hydrogen bonds, with graph set R 2 2(8).

引用

页码：O749 / U2364

页数：8

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