MICROSTRUCTURE OF NANOSILICA MODIFIED BINDER BY ATOMIC FORCE MICROSCOPY

被引:0
作者
Samsudin, Mohamad Saifullah [1 ]
Arshad, Ahmad Kamil [1 ]
Ahmad, Juraidah [1 ]
Masri, Khairil Azman [1 ]
机构
[1] Univ Teknol MARA UITM, Fac Civil Engn, Shah Alam, Selangor, Malaysia
来源
JURNAL TEKNOLOGI | 2016年 / 78卷 / 7-3期
关键词
Nanosilica; atomic force microscopy; scanning electron microscopy; modified binder;
D O I
暂无
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this paper, the effect of nanosilica (NS) on the physical properties as well as aging on the morphology of asphalt binder was investigated. Asphalt binder penetration grade 60/70 (PEN 60/70) was modified with NS at concentrations of 1% to 5% by weight of binder. Scanning electron microscopy (SEM) was used to have a visual evaluation of Nanosilica dispersion. The physical properties tested include is softening point, penetration, ductility, viscosity and storage stability. Temperature susceptibility was evaluated using penetration index (PI) and penetration viscosity number (PVN). Nanosilica modified binder (NSMB) were aged using the rolling thin film oven test (RTFO) and pressure aging vessel (PAV). The morphology of the virgin asphalt binder and NSMB before and after aging was characterized by tapping mode atomic force microscopy (AFM). From the physical properties test, the addition of NS was found to improve the asphalt binder properties and can resist high temperature susceptibility. The results of the AFM imaging showed that the addition of nanosilica in asphalt binder improved its surface stiffness. The overall surface stiffness of the asphalt binder after aging also increased. It can be concluded from this study that 2% to 4% of NS gave the optimum performance for the binder.
引用
收藏
页码:37 / 44
页数:8
相关论文
共 19 条
[1]  
Abdullah ME, 2011, STORAGE STABILITY PH
[2]  
Bahia H. U., 1994, ASTM SPECIAL TECHNIC, V1241
[3]   ATOMIC FORCE MICROSCOPE [J].
BINNIG, G ;
QUATE, CF ;
GERBER, C .
PHYSICAL REVIEW LETTERS, 1986, 56 (09) :930-933
[4]  
Briscoe O. E., 1985, ASPHALT RHEOLOGI REL
[5]   Mechanical properties of asphalt binders evaluated by atomic force microscopy [J].
Dourado, E. R. ;
Simao, R. A. ;
Leite, L. F. M. .
JOURNAL OF MICROSCOPY, 2012, 245 (02) :119-128
[6]  
Jager A., 2004, ROAD MATER PAVEMENT, V5, P9, DOI [DOI 10.1080/14680629.2004.9689985, 10.1080/14680629.2004.9689985]
[7]  
Jones D. R., 1992, UNDERSTANDING ORIGIN, P4
[8]   The colloidal structure of bitumen: Consequences on the rheology and on the mechanisms of bitumen modification [J].
Lesueur, Didier .
ADVANCES IN COLLOID AND INTERFACE SCIENCE, 2009, 145 (1-2) :42-82
[9]   Bitumen in colloid science: a chemical, structural and rheological approach [J].
Loeber, L ;
Muller, G ;
Morel, J ;
Sutton, O .
FUEL, 1998, 77 (13) :1443-1450
[10]   New direct observations of asphalts and asphalt binders by scanning electron microscopy and atomic force microscopy [J].
Loeber, L ;
Sutton, O ;
Morel, J ;
Valleton, JM ;
Muller, G .
JOURNAL OF MICROSCOPY-OXFORD, 1996, 182 (01) :32-39