Microstures of CdC2O4.3H2O Single Crystal Grown in Silica Gel

被引：0

作者：

Shedam, M. R. ^{[1
]}

Shedam, Rakesh M. ^{[2
]}

Mathad, Shridhar N. ^{[3
]}

机构：

[1] New Coll, Shri Padmbhusan DB Patil Res Ctr, Kolhapur, Maharashtra, India

[2] GKG Coll, Dept Phys, Kolhapur 416012, Maharashtra, India

[3] KLEIT, Gokul Rd, Hubballi, Karnataka, India

来源：

JOURNAL OF NANO- AND ELECTRONIC PHYSICS | 2016年 / 8卷 / 04期

关键词：

Surface structure; Overgrowth; Etches pits; Silica gel;

D O I：

10.21272/jnep.8(4(2)).04075

中图分类号：

TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

As part of our work on the growth of cadmium oxalate single crystals in silica gel, an attempt has been made to investigate the growth mechanism of the crystals. This paper deals with the study of surface structures of cadmium oxalate single crystals grown in silica gel. Observation of microstructure is also useful for geologist as crystallization processes in the laboratory have similarities with those in nature. Various growth features such as growth layers as developed etch pits and liquid inclusion have been observed using optical and scanning electron microscopy techniques. Thermal analysis showed that the grown crystals were dehydrated thermally even from lower temperatures. The infrared spectrum (FTIR) revealed the presence of oxalate ligands and water of hydration in both the pure crystals.

引用

页数：4

共 15 条

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