SYNTHESIS OF C-14-LABELED ESCHENMOSER SALT - DIMETHYL([C-14]METHYLENE)AMMONIUM IODIDE

被引：4

作者：

KUPCZYKSUBOTKOWSKA, L ^{[1
]}

SHINE, HJ ^{[1
]}

机构：

[1] TEXAS TECH UNIV,DEPT CHEM & BIOCHEM,LUBBOCK,TX 79409

来源：

JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS | 1993年 / 33卷 / 04期

关键词：

ESCHENMOSER SALT; C-14; IODOFORM; METHYLENE IODIDE;

D O I：

10.1002/jlcr.2580330408

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A six step synthesis of dimethyl([C-14]methylene)ammonium iodide (Eschenmoser's salt) is described. Sodium [2-C-14]acetate was used as the starting material. The overall yield of the final product was 30% with specific activity 8 mCi/mol.

引用

页码：301 / 304

页数：4