Crystal structure of 4,4'-(disulfanediyl)dibutanoic acid-4,4'-bipyridine (1/1)

被引：1

作者：

Maria Atria, Ana ^{[1
]}

Teresa Garland, Maria ^{[2
]}

Baggio, Ricardo ^{[3
]}

机构：

[1] Univ Chile, Fac Ciencias Quim & Farmaceut, Santiago 233, Chile

[2] Univ Chile, Fac Ciencias Fis & Matemat, Dept Fis, Santiago, Chile

[3] Comis Nacl Energi Atom, Ctr Atom Constituyentes, Dept Fis, Buenos Aires, DF, Argentina

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷

关键词：

crystal structure; hydrogen-bonding-disposition; co-crystal;

D O I：

10.1107/S1600536814018558

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

4,4'-(Disulfanediyl) dibutanoic acid (dtba) and 4,4'-bipyridine (4,4'-bpy) crystallize in an 1: 1 ratio, leading to the title co-crystal with composition C8H14O4S2 center dot C10H8N2. A distinctive feature of the crystal structure is the geometry of the dtba moiety, which appears to be stretched [with a 9.98 (1)angstrom span between outermost carbons] and acts as an hydrogen-bonding connector, forming linear chains along [211] with the 4,4'-bpy moiety by way of O-H center dot center dot center dot N hydrogen bonds and C-H center dot center dot center dot O interactions. The influence of the molecular shape on the hydrogen-bonding pattern is analysed by comparing the title compound and two other 4,4'-bpy co-crystals with closely related molecules of similar formulation but different geometry, showing the way in which this correlates with the packing arrangement.

引用

页码：157 / +

页数：9

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