STRUCTURES OF COLCHICINE ANALOGS .5. 2-METHOXY-5-(4-METHOXYPHENYL)CYCLOHEPTA-2,4,6-TRIEN-1-ONE

被引：4
|
作者：
GULBIS, JM [1 ]
MACKAY, MF [1 ]
BANWELL, MG [1 ]
LAMBERT, JN [1 ]
机构：
[1] UNIV MELBOURNE,SCH CHEM,PARKVILLE,VIC 3052,AUSTRALIA
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1992年 / 48卷
关键词：
D O I：
10.1107/S0108270191009411
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
C15H14O3, M(r) = 242.3, monoclinic, Pc, a = 13.219 (1), b = 7.072 (1), c = 6.527 (2) angstrom, beta = 97.23 (1)-degrees, V = 605.3 (3) angstrom 3, Z = 2, D(m) (flotation) = 1.33 (1), D(x) = 1.329 Mg m-3, lambda(Cu K-alpha) = 1.5418 angstrom, mu(Cu K-alpha) = 0.66 mm-1, F(000) = 256, T = 291 (1) K, final R = 0.040 for 905 observed data. The bicyclic molecule adopts a conformation similar to the solid-state conformation of isocolchicine, and the dihedral angle between the planes of the two rings is 41.1 (4)-degrees.
引用
收藏
页码：332 / 334
页数：3
相关论文
共 50 条
  • [21] THE STRUCTURE OF 2-METHOXY-5-(2',3',4'-TRIMETHOXYPHENYL)TROPONE, AN EFFECTIVE ANALOG OF COLCHICINE
    ROSSI, M
    LINK, J
    LEE, JC
    ARCHIVES OF BIOCHEMISTRY AND BIOPHYSICS, 1984, 231 (02) : 470 - 476
  • [22] 5-(4-methoxyphenyl)-1-phenylpyrazolidin-3-one
    Shi, H
    Zhu, HJ
    Yin, PW
    Wang, JT
    Shi, XL
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O2246 - O2247
  • [23] 5-(4-methoxybenzoyl)-4-(4-methoxyphenyl)-1-[1-(4-methoxyphenyl)ethylidenenamino]pyrimidin-2(1H)-one
    Özçelik, S
    Dinçer, M
    Saripinar, E
    Yilmaz, C
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O637 - O638
  • [24] 5-(4-methoxybenzoyl)-4-(4-methoxyphenyl)-1-[1-(4-methoxyphenyl)ethylideneamino]-pyrimidin-2(1H)-one
    Özçelik, S
    Dinçer, M
    Saripinar, E
    Yilmaz, Ç
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O622 - O624
  • [25] 5-Hydroxy-7-methoxy-2-(4-methoxyphenyl)-4H-1-benzopyran-4-one (vol 61, pg 3715, 2005)
    Teh, JBJ
    Fun, HK
    Razak, IA
    Chantrapromma, S
    Boonnak, N
    Karalai, C
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : E9 - E9
  • [26] Electrochemically Induced Transformations of Tetrabrominated 2-Dibromomethyl-2-methylcyclohexan-1-one and Its Brominated Unsaturated Analogs into 2-Methylcyclohepta-2,4,6-trien-1-one
    Moiseeva, A. A.
    Gavrilova, G. V.
    Krutko, D. P.
    Beloglazkina, E. K.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2019, 89 (06) : 1183 - 1189
  • [27] Electrochemically Induced Transformations of Tetrabrominated 2-Dibromomethyl-2-methylcyclohexan-1-one and Its Brominated Unsaturated Analogs into 2-Methylcyclohepta-2,4,6-trien-1-one
    A. A. Moiseeva
    G. V. Gavrilova
    D. P. Krutko
    E. K. Beloglazkina
    Russian Journal of General Chemistry, 2019, 89 : 1183 - 1189
  • [28] 3,5,7-Trimethoxy-2-(4-methoxyphenyl)-4H-1-benzopyran-4-one
    Aree, Thammarat
    Sawasdee, Pattara
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O2706 - U382
  • [29] 5-METHOXY-2-(2-METHOXYPHENYL)-4H-1-BENZOPYRAN-4-ONE (2,5'-DIMETHOXYFLAVONE)
    WALLET, JC
    GAYDOU, EM
    TINANT, B
    DECLERCQ, JP
    BALDY, A
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1992, 48 : 376 - 377
  • [30] Crystal structures and Hirshfeld surface analysis of 5-amino-1-(4-methoxyphenyl)pyrazole-4-carboxylic acid and 5-amino-3-(4-methoxyphenyl)-isoxazole
    Pintro, Chris J.
    Long, Analeece K.
    Amonette, Allison J.
    Lobue, James M.
    Padgett, Clifford W.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2022, 78 : 336 - +
12345