THE CRYSTAL-STRUCTURE OF SOLID PERRHENIC ACID MONOHYDRATE

被引：12
|
作者：
WLTSCHEK, G [1 ]
SVOBODA, I [1 ]
FUESS, H [1 ]
机构：
[1] TH DARMSTADT,FACHBEREICH MAT WISSENSCH,PETERSENSTR 20,W-6100 DARMSTADT,GERMANY
来源：
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE | 1993年 / 619卷 / 10期
关键词：
PERRHENIC ACID; HREO4.H2O; CRYSTAL STRUCTURE; SYNTHESIS;
D O I：
10.1002/zaac.19936191007
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Solid perrhenic acid monohydrate has been characterized by X-ray single crystal structure analysis (300 K). HReO4 . H2O, M(r) = 269.23, tetragonal, 14(1)/a, Scheelite-type (CaWO4), a = 5.8320(2) angstrom, c = 12.9384(6) angstrom, V = 440.06(5) angstrom3, Z = 4, D(x) = 4.063 g cm-3, X-ray wavelength lambda (MoKalpha) = 0.71069 angstrom. The structure consists of [ReO4]--tetrahedra and oxonium ions linked by hydrogen bridges to form a three-dimensional network.
引用
收藏
页码：1679 / 1681
页数：3
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