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- [21] catena-Poly[[aquabis[N-(pyridin-3-yl)-isonicotinamide-kappa N-1]copper(II)]-mu-fumarato-kappa O-2(1):O-4]ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : M1514 - +Qiblawi, Sultan H.LaDuca, Robert L.
N-(2-Fluorobenzyloxy)-1,3,5-trimethyl-2,6-diphenylpiperidin-4-imine
被引：0
作者：
Ramalingan, Chennan
[1
]
Ng, Seik Weng
[2
,3
,4
]
Tiekink, Edward R. T.
[2
]
机构：
[1] Kalasalingam Univ, Ctr Nanotechnol, Dept Chem, Krishnankoil 626126, Tamil Nadu, India
[2] Univ Malaya, Dept Chem, Kuala Lumpur 50603, Malaysia
[3] King Abdulaziz Univ, Chem Dept, Jeddah, Saudi Arabia
[4] King Abdulaziz Univ, Fac Sci, Jeddah, Saudi Arabia
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS
|
2012年
/
68卷
关键词：
data-to-parameter ratio = 9.6;
mean σ(C-C) = 0.004 Å;
R factor = 0.041;
single-crystal X-ray study;
T = 100 K;
wR factor = 0.101;
D O I：
10.1107/S1600536812029327
中图分类号：
O7 [晶体学];
学科分类号：
0702 ;
070205 ;
0703 ;
080501 ;
摘要：
In the title compound, C27H29FN2O, the piperidine ring has a twisted boat conformation and all ring substituents occupy equatorial positions. The dihedral angle formed between the phenyl rings is 66.71 (12)degrees, and the phenyl rings form dihedral angles of 46.60 (13) and 43.75 (13)degrees with the fluorobenzene ring, which occupies a position coplanar to the methoxy(methylidene) amine residue [N-O-C-C torsion angle = -179.5 (2)degrees]. In the crystal, a complex network of C-H center dot center dot center dot pi interactions connects the molecules into a three-dimensional architecture.
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页码：02312 / +
页数：11
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