SUPERCRITICAL-FLUID CHROMATOGRAPHY OF PETROLEUM-PRODUCTS USING FLAMELESS SULFUR CHEMILUMINESCENCE DETECTION

被引：0
作者：
SHEARER, RL
SKELTON, RJ
机构：
来源：
HRC-JOURNAL OF HIGH RESOLUTION CHROMATOGRAPHY | 1994年 / 17卷 / 04期
关键词：
SULFUR ANALYSIS; PETROLEUM PRODUCTS; SULFUR CHEMILUMINESCENCE DETECTION; PACKED COLUMNS; SUPERCRITICAL FLUID CHROMATOGRAPHY;
D O I：
暂无
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Supercritical fluid chromatography using flameless sulfur chemiluminescence detection has been investigated for the analysis of sulfur compounds in petroleum products. The chromatography and detection system was easy to implement and exhibited good precision, linearity, selectivity, and sensitivity. A minimum detectable limit of 0.3 pg sulfur/s was obtained, and response to sulfur in different sulfur species was nearly equimolar.
引用
收藏
页码：251 / 254
页数：4
相关论文
共 9 条
[1]   USE OF PACKED-COLUMN SUPERCRITICAL FLUID CHROMATOGRAPHY WITH OZONE-BASED SULFUR CHEMILUMINESCENCE DETECTION [J].
HOWARD, AL ;
TAYLOR, LT .
ANALYTICAL CHEMISTRY, 1993, 65 (06) :724-729
[2]   EVALUATION OF A SUPERCRITICAL FLUID CHROMATOGRAPH COUPLED TO A SURFACE-WAVE-SUSTAINED MICROWAVE-INDUCED PLASMA DETECTOR [J].
LUFFER, DR ;
GALANTE, LJ ;
DAVID, PA ;
NOVOTNY, M ;
HIEFTJE, GM .
ANALYTICAL CHEMISTRY, 1988, 60 (14) :1365-1369
[3]   CHARACTERIZATION AND OPTIMIZATION OF FLAME PHOTOMETRIC DETECTION IN SUPERCRITICAL FLUID CHROMATOGRAPHY [J].
OLESIK, SV ;
PEKAY, LA ;
PALIWODA, EA .
ANALYTICAL CHEMISTRY, 1989, 61 (01) :58-65
[4]   SUPERCRITICAL FLUID CHROMATOGRAPHY FLAME PHOTOMETRIC DETECTION - DETERMINATION OF HIGH MOLECULAR-WEIGHT COMPOUNDS [J].
PEKAY, LA ;
OLESIK, SV .
ANALYTICAL CHEMISTRY, 1989, 61 (23) :2616-2624
[5]  
PEKAY LA, 1990, J MICROCOLUMN SEP, V2, P270
[6]   DEVELOPMENT OF FLAMELESS SULFUR CHEMILUMINESCENCE DETECTION - APPLICATION TO GAS-CHROMATOGRAPHY [J].
SHEARER, RL .
ANALYTICAL CHEMISTRY, 1992, 64 (18) :2192-2196
[7]   APPLICATION OF GAS-CHROMATOGRAPHY AND FLAMELESS SULFUR CHEMILUMINESCENCE DETECTION TO THE ANALYSIS OF PETROLEUM-PRODUCTS [J].
SHEARER, RL ;
POOLE, EB ;
NOWALK, JB .
JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1993, 31 (03) :82-87
[8]  
SKELTON RJ, 1989, ANAL CHEM, V61, P1813
[9]  
SUE WF, 1992, CHROMATOGRAPHIA, V33, P507
1