CHEMICAL-STRUCTURE OF THE CORE REGION OF CAMPYLOBACTER-JEJUNI SEROTYPE O-2 LIPOPOLYSACCHARIDE

被引：74
作者：
ASPINALL, GO
MCDONALD, AG
RAJU, TS
PANG, H
KURJANCZYK, LA
PENNER, JL
MORAN, AP
机构：
[1] UNIV TORONTO,DEPT MOLEC & MED GENET,CARBOHYDRATE RES CTR,TORONTO M5S 1A1,ONTARIO,CANADA
[2] UNIV TORONTO,DEPT MICROBIOL,TORONTO M5S 1A1,ONTARIO,CANADA
[3] NATL UNIV IRELAND UNIV COLL GALWAY,DEPT MICROBIOL,GALWAY,IRELAND
来源：
EUROPEAN JOURNAL OF BIOCHEMISTRY | 1993年 / 213卷 / 03期
关键词：
D O I：
10.1111/j.1432-1033.1993.tb17850.x
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
The complete structure for the core region of Campylobacter jejuni serotype O:2 lipopolysaccharide (LPS) was assigned through studies on derivatives of the liberated oligosaccharide (OS 2) and the intact LPS. Structure determinations were performed using H-1-NMR spectroscopy, methylation studies supported by fast-atom-bombardment mass spectrometry and linkage analysis by gas chromatography/mass spectrometry, Smith degradation, and oxidation with chromium trioxide. It was concluded that complete oligosaccharide chains had the following structure: [GRAPHICS]
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页码：1029 / 1037
页数：9
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